Sciencemadness Discussion Board

Inexpensive Distillation Equipment

DFliyerz - 8-1-2015 at 09:54

I have a hot plate with a rest for a boiling flask already, but where could I get the rest of the required equipment such as a boiling flask, condenser, the required tubing, etc. for under $75?

Bert - 8-1-2015 at 10:03

http://www.ebay.com/bhp/distillation-kit

Mailinmypocket - 8-1-2015 at 10:05

I've ordered from these guys a few times and have been very impressed. Even delicate items like the high efficiency reflux condensers are well built and have never failed me. Once they sent me a 90 degree takeoff adapter when I was supposed to get a vacuum take off adapter. No problem! They sent me the proper item and let me keep the other one.

http://www.laboyglass.com

DFliyerz - 8-1-2015 at 10:10

Quote: Originally posted by Bert  
http://www.ebay.com/bhp/distillation-kit


Some of those kits with the clips to hold the parts together look like they'd be ideal and inexpensive. Can they support their own weight, or would I have to buy some equipment to hold them up?

Mailinmypocket - 8-1-2015 at 10:20

Keck clips are not intended to support weight, only to keep joints together. Sometimes you can support a very small flask on the end of a condenser with one but for anything remotely heavy you would want a couple clamps and stands

Bert - 8-1-2015 at 10:33

You need supports to use those safely- Stands, rods, clamps.

Go read up on the operation before ordering- This saves on equipment replacement costs, ER visits, legal expenses...

image.jpg - 78kB

chemrox - 8-1-2015 at 17:44

Thanks for the laughs everyone. You can get self supporting hillbilly stills too.

j_sum1 - 8-1-2015 at 20:18

My distillation condenser is a two foot liebig that I jury-rigged out of a broken burette, some plastic hose and some epoxy putty. I haven't put it through its paces yet but it operated well for reflux. It's a stand-in for until I have the bucks to afford a proper rig. (Or more likely until I break it and decide I really can't do without it.)
My stand is some concrete reinforcing mesh that I have installed on the bench in my shed. It cost nearly nothing. I did buy some proper boss head clamps, some retort rings and some three finger clamps. I wouldn't recommend skimping here. Having stuff stay where you want it reliably is a real bonus.