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Author: Subject: Red phosphorus to Phosphorus trichloride?
ErgoloidMesylate
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[*] posted on 11-5-2023 at 11:42


Quote: Originally posted by Tsjerk  
If that patent would be interesting that might be fine, but you don't provide a source.


Years before this thread was started, several different posters here mentioned this route.

One place online that still has the procedure is here.

It claims to make a mixture, of phosphorus halides and phosphorus oxyhalides.

https://archive.org/details/Phosphorus_oxychloride_from_calc...




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clearly_not_atara
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[*] posted on 11-5-2023 at 13:15


Quote:
This mixture is heated to 500-600 C while a stream of chlorine is passed over it
Can't imagine why that didn't catch on.



Quote: Originally posted by bnull  
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ErgoloidMesylate
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[*] posted on 11-5-2023 at 14:59


Quote: Originally posted by clearly_not_atara  
Quote:
This mixture is heated to 500-600 C while a stream of chlorine is passed over it
Can't imagine why that didn't catch on.


Maybe you should stop hanging around chemistry places if temperature variety is going to dissuade you.




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