Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Printable Version  
Author: Subject: Chromium from thermite
Foeskes
Hazard to Others
***




Posts: 156
Registered: 25-2-2017
Member Is Offline

Mood: No Mood

[*] posted on 22-9-2017 at 17:51
Chromium from thermite


I recently made chromium from thermite.
The recipe I used was 20 grams Cr2O3:12 grams K2Cr2O7:11.4 grams Aluminium powder.
The mixture was ignited using some magnesium ribbon and a mixture of aluminium and sulfur.
After breaking the slag I got around 12 grams of chromium(~67% yield based on Cr2O3 and K2Cr2O7) although it likely contains Al contamination like most thermite reactions.

(The remaining slag and the thermite container was put in a ascorbic acid solution to destroy any Cr(VI) )

[Edited on 23-9-2017 by Foeskes]

image.jpeg - 1.9MB

[Edited on 23-9-2017 by Foeskes]

image.jpeg - 1.9MB

[Edited on 23-9-2017 by Foeskes]
View user's profile View All Posts By User
j_sum1
Administrator
********




Posts: 6321
Registered: 4-10-2014
Location: At home
Member Is Offline

Mood: Most of the ducks are in a row

[*] posted on 22-9-2017 at 18:02


Rather nice.
I would love to see a cut or ground surface to see if you get the characteristic shiny that Cr exhibits.
View user's profile View All Posts By User
Foeskes
Hazard to Others
***




Posts: 156
Registered: 25-2-2017
Member Is Offline

Mood: No Mood

[*] posted on 22-9-2017 at 18:54


When breaking the slag the were small beads of chromium and after breaking one, it was pretty shiny. It looks kinda similar to the attached image, but smaller.

[Edited on 23-9-2017 by Foeskes]

image.jpeg - 33kB
View user's profile View All Posts By User

  Go To Top