highuse
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acetylsalicylic acid + H2SO4 ==> phenols
Hello I am a french student in second year of chemistry in university, I have make some work on explosive substance and for the picric acid i take an
synthesis with acetylsalicylic acid !
i have a bad document about some bad cook ( i don't use it for cook but just by the chemical interest ! )
and in the synthesis it's explain, H2SO4 use on acetylsalicylic acid can cut the COOH and OCOCH3 and to form finaly phenol, but i don't understand
exatly how mechanism work ! so if some one can make me a draw of the mechanism and some explication it's can be magic 
I think i fall in love to this forum when i see a discution about TATP, cook some explosive  ect.... in french forum if you just talk about H2SO4 or HNO3 the topic have great chance to be close :/
[Edited on 11-3-2015 by highuse]
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Pasrules
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Here is some information on the hydrolysis of esters http://www.chem.ucalgary.ca/courses/351/Carey5th/Ch20/ch20-3...
Also it would help if you could post your said document.
[Edited on 11-3-2015 by Pasrules]
Atropine, Bicarb, Calcium.
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highuse
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a great thanks for the link !!
LOL post the exact cook of TNT · Nitroglycérine · TNP · PETN Tétranitrate) · RDX · Plastics (B, C1, C4, Semtex) · HMX · Chlorate de Soude
· Peroxyde d'Acétone · Nitrocellulose · Fulminate de Mercure · Nitrure de Plomb · Triiodure d'Azote · Hexal · HMTD
it's illegal in my country, show on internet can give me 3 year in prison and 45 000€, and i think you know about some event in my country and "red
alert" for terrorism so i'm not to hot with the idea to give cook of explosive now ^^
[Edited on 11-3-2015 by highuse]
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Bert
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Quote: Originally posted by highuse  | a great thanks for the link !!
LOL post the exact cook of TNT · Nitroglycérine · TNP · PETN Tétranitrate) · RDX · Plastics (B, C1, C4, Semtex) · HMX · Chlorate de Soude
· Peroxyde d'Acétone · Nitrocellulose · Fulminate de Mercure · Nitrure de Plomb · Triiodure d'Azote · Hexal · HMTD
[Edited on 11-3-2015 by highuse] |
It would be called "synthesis" around here. Cooking is done in a kitchen... Or possibly a meth lab.
Anyhow, welcome to the board.
Please read the sciencemadness.org FAQ.
These are not exactly cookbooks-
Not familiar with EU/French law. Could you post a link to the statutes? There have certainly been French and Belgian members posting on explosives
here in the past.
Rapopart’s Rules for critical commentary:
1. Attempt to re-express your target’s position so clearly, vividly and fairly that your target says: “Thanks, I wish I’d thought of putting it
that way.”
2. List any points of agreement (especially if they are not matters of general or widespread agreement).
3. Mention anything you have learned from your target.
4. Only then are you permitted to say so much as a word of rebuttal or criticism.
Anatol Rapoport was a Russian-born American mathematical psychologist (1911-2007).
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Pasrules
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Actually i am french aswell but i live in Australia, the news has been bad so i can imagine the laws. I suggest if want you are interested in may put
you at risk then use a VPN for your search services.
Also here a book on the preparation of this compound from aspirin Prep manual of explosives
Here is one extra link for the prep which i will post the mechanism below
[Edited on 12-3-2015 by Pasrules]
Atropine, Bicarb, Calcium.
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highuse
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thx for the help
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