Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Printable Version  
Author: Subject: precipitating ppa hcl help
luna
Harmless
*




Posts: 1
Registered: 29-11-2014
Member Is Offline

Mood: No Mood

[*] posted on 8-2-2015 at 23:11
precipitating ppa hcl help


Could someone here help me? I have situation where i attemp the akabori reaction based on Quantum Dom post. First when i adding sodium carbonate and NaOH granules then i got brown oily layer on top of aqueous phase.
This oil was solidified when separatey question is
Can i just throw this oil onto acetone and titrate it? Or should i disolve it on dcm then distill the dcm first then i titrating it? I ever try with methode disolve on dcm and wash with brine and distil the dcm . What left is viscous oil, and i add aceton on that oil then titrate until ph4 but i didnt get anything leftt on acetone after titrating. Any sugestion for me ? Thank you and sory about bad language
View user's profile View All Posts By User
Nicodem
Super Moderator
Thread Moved
8-2-2015 at 23:49

  Go To Top