arkoma
Redneck Overlord
Posts: 1763
Registered: 3-2-2014
Location: On a Big Blue Marble hurtling through space
Member Is Offline
Mood: украї́нська
|
|
First SUCCESSFUL steam distillation
Well, I tried and tried and tried to generate enough steam in an oil bath (I hava a HUGE fear of fires) but it just didna work. So I appropriated my
sisters teapot (shhhhhhb!!!!!) and used the gas side burner on the BBQ grill. I actually ended upwith a visible amount of basil oil w00t w00t!!
Steam adapter:
LOTS of PTFE tape
In the thermometer adapter/stillhead
FAIL steam generator
OMG, some drunk swiped my sisters tea kettle
slightly reamed out the whistler hole--hopefully she doesn't catch me (it still whistles)
Can't really see it, but there isa layer of sweet basil oil on top of the H2O
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
|
|
violet sin
International Hazard
Posts: 1480
Registered: 2-9-2012
Location: Daydreaming of uraninite...
Member Is Offline
Mood: Good
|
|
Nice work man, I have been really wanting to get distilling with steam my self. What all do you have planned? The possibilities are many. I started
a big planter if mint just for this, saved a gallon bag of Orange blossoms, 1.5gal of lemon zest and have orange peels, grapefruit peels, access to
annise, basil, parsley and more. Not from stores, home grown.
Looks to be a lot of fun. Can't wait to get started, but in the meantime time, keep posting. I find this subject interesting
|
|
hyfalcon
International Hazard
Posts: 1003
Registered: 29-3-2012
Member Is Offline
Mood: No Mood
|
|
I've got a 6 X 30' patch of lemon balm I've been wanting to do this to. I've obviously got to scale up for mine though.
|
|
arkoma
Redneck Overlord
Posts: 1763
Registered: 3-2-2014
Location: On a Big Blue Marble hurtling through space
Member Is Offline
Mood: украї́нська
|
|
I've got some pine gathered up and also some Encelia Turns out there is an intertesting looking benzaldehyde in the encelia.
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
|
|
Loptr
International Hazard
Posts: 1348
Registered: 20-5-2014
Location: USA
Member Is Offline
Mood: Grateful
|
|
Title: 5-Acetyl-2-methoxybenzaldehyde
CAS Registry Number: 531-99-7
Additional Names: 3-Acetyl-6-methoxybenzaldehyde
Molecular Formula: C10H10O3
Molecular Weight: 178.18
Percent Composition: C 67.41%, H 5.66%, O 26.94%
Literature References: A natural plant growth inhibitor found in the leaves of Encelia farinosa A. Gray, Compositae. Isoln and synthesis from
3-acetyl-6-methoxybenzonitrile: Gray, Bonner, J. Am. Chem. Soc. 70, 1249 (1948).
Properties: Needles from alcohol or ether, mp 144°. Sublimes without decomp. Emits fragrant odor on prolonged heating. Sol in hot water, warm ether,
alcohol, benzene, chloroform. Practically insol in cold water, 5% HCl, 5% NaOH, petr ether, carbon tetrachloride. Sol with orange color in concd
mineral acids.
Melting point: mp 144°
|
|
hyfalcon
International Hazard
Posts: 1003
Registered: 29-3-2012
Member Is Offline
Mood: No Mood
|
|
I thing black walnut has a similar growth inhibiting substance in it.
http://www.wvu.edu/~agexten/hortcult/fruits/blkwalnt.htm
|
|
aga
Forum Drunkard
Posts: 7030
Registered: 25-3-2014
Member Is Offline
|
|
Neat.
Kettle as a steam generator.
Wish i had thought of that !
|
|
arkoma
Redneck Overlord
Posts: 1763
Registered: 3-2-2014
Location: On a Big Blue Marble hurtling through space
Member Is Offline
Mood: украї́нська
|
|
I tried using a canning jar with pipe soldered to lid in oil bath at first FAIL.
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
|
|