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Author: Subject: Ehylene-diamine cellulose synthesis
rodanid88
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[*] posted on 16-7-2012 at 13:21
Ehylene-diamine cellulose synthesis


My question is that, what is the name or mechanism of these reactions?
I know the description of the reaction only. So the first step:
Cellulose powder + POCl3 + dimethylformamide stirring and heating for 20 minutes and 90 C degrees. After that, filtration and washing of the cellulose.
The second reaction: The washed and dry cellulose react with ethylene-diamine and form ehylene-diamine cellulose.
Thank you,
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zoombafu
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[*] posted on 16-7-2012 at 13:40


What are you referencing this synthesis from?



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rodanid88
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[*] posted on 16-7-2012 at 13:51


Quote: Originally posted by zoombafu  
What are you referencing this synthesis from?


We have prepared it at the university, but i dont know nothing more about it unfortunately. only that, the dimethylformamide is the solvent.I have annexed the equation of the reaction.

1-s2.0-S0304389405005194-gr2.jpg - 22kB
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Nicodem
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[*] posted on 17-7-2012 at 11:51


Quote: Originally posted by rodanid88  
My question is that, what is the name or mechanism of these reactions?

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