andre178
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Location: San Diego, CA
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Setting up microwave for chemistry
I have a used microwave that I can use for chemistry, in the chemical hood or outside, I was wondering if there are any cautions on using it. Is it
chemical ready? is ventilation sufficient for it not to explode? Any advice on this.
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franklyn
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Thanks to solo for this _
Modification of a commercial microwave Oven for applications in the chemical laboratory
http://www.sciencemadness.org/talk/files.php?pid=83638&a...
not_important provided these links _
http://home.c2i.net/metaphor/mvpage.html
http://www.animations.physics.unsw.edu.au/jw/superheating.ht...
2 continuous power levels - not intermitant on / off
http://www.sciencemadness.org/talk/viewthread.php?tid=11184#...
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smaerd
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why don't I have permission to view the first link? This is something I am definitely interested in!(sorry to de-rail thread if I did).
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andre178
Hazard to Self
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I can't see it either, and I searched for it w/o success
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Formatik
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I've used a regular household microwave to dry mostly inorganic salts, like acetates, chlorides, oxides and hydroxides with good results. But I drive
off most of the water by heating under a flame or hotplate beforehand. Water-wet calcium hydroxide in the microwave started to catch on fire (!). This
didn't happen if the salt was mostly dehydrated by heating beforehand. Doing that, I've had no problems heating for a few short minutes. I will use it
only if I need something anhydrous.
[Edited on 23-7-2010 by Formatik]
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zed
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Microwave Assisted Organic Synthesis (Hardcover)
by Jason P. Tierney (Author), Pelle Lidstrom (Author)
Looks like a good book on the subject. Google will give you a free look-see.
http://books.google.com/books?id=zG7AbALcNigC&pg=PA266&a...
If you happen to be in the UK, someone is offering a nice copy for only Seven Dollars and Eighty Four cents...On Amazon.
Were I there, I would buy it. Me, being in the US., creates an expensive "Postage Barrier".
http://www.amazon.com/gp/search?index=books&linkCode=qs&...
[Edited on 5-8-2010 by zed]
[Edited on 5-8-2010 by zed]
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franklyn
International Hazard
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There are more than one publications , books and articles with this title
Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures - Dariusz Bogdal
http://books.google.com/books?id=9KcZUVZix08C&lpg=PP1&am...
Microwave Assisted Organic Synthesis - Jason P. Tierney, Pelle Lidström
http://books.google.com/books?id=zG7AbALcNigC&lpg=PP1&am...
Both available in the references section => go there
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un0me2
aliced25 sock puppet
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Has anyone got anything on the dehydration of Calcium Hydroxide to Calcium Oxide in the MW? Now that would be a useful reaction, especially if
lithium, potassium or sodium hydroxide mixtures could be calcined in the mixture. That should give the relevant oxides (as other heating methods are
claimed to do on mixtures of the same with Ca(OH)2 are supposed to achieve), which would be phenomenal in
producing the alkali metal alkoxides - the hydration of the oxides would remove a shitload of water (that produced by the reaction) at the outset.
quam temere in nosmet legem sancimus iniquam
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