Quote: Originally posted by Formatik  | | Quote: | Originally posted by Taoiseach
urea with acetic acid
Is acetic anhydride necessary for this reaction to work? |
No, I don't think so. Gmelin says heating urea with AcOH to 110 deg.C. forms acetamide, pitty nothing further like reaction time, extraction, etc. but
they reference: M.T. Dangyan (Bull. Armenian Branch Acad. USSR 1942 No. 9/10 (23/4), pg. 53/72), C.A. 1946 3399, and
J.M. Das-Gupta (J. Indian Chem. Soc. 10 [1933] 117/23). These references, especially the first should have more details about this
process. |
Studies on the Decompositions and Reactions of Urea.Part II. Reactions of Urea with Acids , Anhydrides, etc.
By Jnanendra Mohon Das-Gupta.
J. Indian Chem. Soc. 10 [1933] 117
Attachment: 10_1933-113-119.pdf (194kB)
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