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Author: Subject: Hydroiodic acid and sodium ethoxide/butoxide sources
argox120
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[*] posted on 4-10-2024 at 10:48
Hydroiodic acid and sodium ethoxide/butoxide sources

would like to get my hands on these reagents"
Hydroiodic acid(250-500ml) and sodium ethoxide or sodium tertbutoxide(100g-250g) for a reduction of teriary alcohol.
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Sir_Gawain
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[*] posted on 4-10-2024 at 17:58


Are you unable to make them yourself? That’s likely going to be easier than buying.



“Alchemy is trying to turn things yellow; chemistry is trying to avoid things turning yellow.” -Tom deP.
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j_sum1
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[*] posted on 4-10-2024 at 22:48


Duplicate thread. I am closing the other one.
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bnull
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[*] posted on 5-10-2024 at 05:38


There are other routes available that don't make use of HI or EtONa. What tertiary alcohol is it?



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argox120
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[*] posted on 5-10-2024 at 08:42


it is a benzylic tertiary alchol like 1,1 dimethyl benzyl alcohol
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bnull
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[*] posted on 5-10-2024 at 12:34


2-phenyl‐2-propanol, eh? Trying to make cumene and analogues?

What about generating HI in situ?

I remember seeing something for tertiary alcohols, like a Wolff-Kischner. Are you following a published procedure?

I ask those questions because there're probably other ways that don't need HI or EtONa.



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[*] posted on 5-10-2024 at 12:51


Does it need to be Sodium Ethoxide or can Magnesium Ethoxide be used?
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thermochromic
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[*] posted on 9-11-2024 at 19:06


Just make the HI... your not going to find a legit company willing to sell it to you... either in situ or there is a super easy synth over on Rhodium
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