Sidertenebris
Harmless
Posts: 3
Registered: 14-9-2016
Member Is Offline
Mood: No Mood
|
|
Chemistry Projects
Hello,
For my extra science class me and my friends need to choose a project. Our school has most of the basic materials, but nothing too fancy. We are in
11th grade and we have never worked in a lab before. The project has to take a school year. The subject should be chemistry, or maybe biochemistry, as
long as it's not too dangerous. We need to make a list of fifty possible projects so any ideas would be welcome. Does anyone know a
project/experiment?
Thank you very much!!!!
|
|
Texium
Administrator
Posts: 4581
Registered: 11-1-2014
Location: Salt Lake City
Member Is Offline
Mood: PhD candidate!
|
|
Fifty possible projects each potentially lasting a school year, or fifty projects which together would fill a school year?
Last year when I was a senior in high school I had an independent study chemistry period in which I was basically allowed free reign in one of the
school's labs. I had a similar idea of coming up with a project that I could work on throughout the year, or at least for a few months before choosing
something else. I quickly realized though that the ideas for projects that I had usually ended up not working out or would be more practical to do in
my lab at home due to limited time at school despite the superior supplies. Because of this I shifted between small projects a lot.
Basically what I'm saying is don't sign onto one project idea and hand it in with the expectation that you will work on it all year. It's simply not
realistic.
To suggest ideas, we'll need to know more about you and what your knowledge, skill, and interest levels are. You say you've never worked in a lab
before, but have you at least taken high school chemistry? When you say the subject "should" be chemistry, does that mean that you want it to be
chemistry or your teacher told you it has to be chemistry?
|
|
Sidertenebris
Harmless
Posts: 3
Registered: 14-9-2016
Member Is Offline
Mood: No Mood
|
|
I would think so too: I really can't find any experiments that take a year. Take in mind I only have two hours a week, so maybe in that way it would
take a year? Things that students did were brewing beer, or making ferrofluids. I have had two years of chemistry (first one hour, then two) but only
theoretical, so we don't have any experience of actually doing experiments. We want to do chemistry, partly because we want to acquire more
experience, partly because we think it would be more fun.
|
|
MrHomeScientist
International Hazard
Posts: 1806
Registered: 24-10-2010
Location: Flerovium
Member Is Offline
Mood: No Mood
|
|
You could join the ranks of people here processing hard drive magnets for interesting chemicals. See the stickied thread: http://www.sciencemadness.org/talk/viewthread.php?tid=14145
It's certainly taken me over a year (years?), mostly because I get quickly distracted by other interesting things. Heck it might even take you a year
to read the thread!
The supplies are reasonably easy to source: magnets, H<sub>2</sub>SO<sub>4</sub>,
K<sub>2</sub>SO<sub>4</sub>, and KOH to isolate the Nd. Depending on how far you want to take it, it gets harder and more
dangerous after that.
[Edited on 9-14-2016 by MrHomeScientist]
|
|
Sidertenebris
Harmless
Posts: 3
Registered: 14-9-2016
Member Is Offline
Mood: No Mood
|
|
I think I'm going to put it on the list. Looks quite interesting, I'll need to ask my chemistry teacher about it though, since English isn't my native
language...
|
|
MrHomeScientist
International Hazard
Posts: 1806
Registered: 24-10-2010
Location: Flerovium
Member Is Offline
Mood: No Mood
|
|
The final steps I definitely would not recommend for you - they involve highly dangerous fluorides and high temperature reactions in special
apparatus. But you can certainly separate the various compounds in a magnet into interesting and colorful chemicals! Seeing Nd salts change color in
different types of lighting is very cool.
|
|
Sulaiman
International Hazard
Posts: 3696
Registered: 8-2-2015
Location: 3rd rock from the sun
Member Is Offline
|
|
since you have a long time but short weekly sessions
I imagine that best use of time could be;
. crystal growing
. fermentation (possibly some distillation also)
. germination
. biological growth
. biological life cycles
and what conditions influence the above.
First choice based on
. which actually interests you
. which is most likely to give good grades
. learning a useful skill; brewing, distilling, planting, growing are all useful in different ways.
CAUTION : Hobby Chemist, not Professional or even Amateur
|
|
crystal grower
Hazard to Others
Posts: 474
Registered: 3-1-2016
Location: Os Petrosum
Member Is Offline
Mood: Puzzled
|
|
Crystal growing is a great stuff! Just remeber not to stick only to blue vitriol (even from copper sulfate one can crystallize 4 hydrates and
anhydrate too).
|
|
DraconicAcid
International Hazard
Posts: 4333
Registered: 1-2-2013
Location: The tiniest college campus ever....
Member Is Offline
Mood: Semi-victorious.
|
|
Quote: Originally posted by crystal grower | Crystal growing is a great stuff! Just remeber not to stick only to blue vitriol (even from copper sulfate one can crystallize 4 hydrates and
anhydrate too). |
How do you crystallize anhydrous CuSO4?
Please remember: "Filtrate" is not a verb.
Write up your lab reports the way your instructor wants them, not the way your ex-instructor wants them.
|
|
Sulaiman
International Hazard
Posts: 3696
Registered: 8-2-2015
Location: 3rd rock from the sun
Member Is Offline
|
|
from methanol, or anhydrous HOH ?
EDIT: http://chemister.ru/Database/properties-en.php?dbid=1&id...
[Edited on 14-9-2016 by Sulaiman]
Also, it now occurs to me that there is relatively little anhydrous inorganic chemistry material ... AHA ! I thought, an area for me to investigate,
then I realised how tedious anhydrous chemistry must be ... no thanks !
But if practical, the growing of anhydrous crystals of compounds that are normally only seen as a hydrate may be an interesting project ?
[Edited on 14-9-2016 by Sulaiman]
CAUTION : Hobby Chemist, not Professional or even Amateur
|
|
crystal grower
Hazard to Others
Posts: 474
Registered: 3-1-2016
Location: Os Petrosum
Member Is Offline
Mood: Puzzled
|
|
Frankly, I haven't tried it yet, but I will certainly try it in near future.
It is possible to make (small) crystals of anhydrous cuso4 via crystallization from hot fuming sulfuric acid (it should be possible with concentrated
H2SO4 too). I can give you a link to the article where the experiment is described if you want.
It isn't as simple as crystallization of blue vitriol of course but it is very
interesting experiment IMO.
|
|
MrHomeScientist
International Hazard
Posts: 1806
Registered: 24-10-2010
Location: Flerovium
Member Is Offline
Mood: No Mood
|
|
I'd definitely like to read about that!
|
|
crystal grower
Hazard to Others
Posts: 474
Registered: 3-1-2016
Location: Os Petrosum
Member Is Offline
Mood: Puzzled
|
|
Ok, I'll post the link tomorrow when I get to my computer.
|
|
Sulaiman
International Hazard
Posts: 3696
Registered: 8-2-2015
Location: 3rd rock from the sun
Member Is Offline
|
|
Although according to the reference that I posted the solubility of anhydrous CuSO4 in methanol at 45 C is only 2.99 g/100g,
it would be safer than boiling H2SO4
and
with a little research, better anhydrous solvents probably can be found.
There must be a plethora of anhydrous compound/solvent mixtures to try.
CAUTION : Hobby Chemist, not Professional or even Amateur
|
|
DraconicAcid
International Hazard
Posts: 4333
Registered: 1-2-2013
Location: The tiniest college campus ever....
Member Is Offline
Mood: Semi-victorious.
|
|
Quote: Originally posted by Sulaiman | Although according to the reference that I posted the solubility of anhydrous CuSO4 in methanol at 45 C is only 2.99 g/100g,
it would be safer than boiling H2SO4
and
with a little research, better anhydrous solvents probably can be found.
There must be a plethora of anhydrous compound/solvent mixtures to try. |
The trouble with anhydrous solvents for dissolving such compounds that most of them a) will not dissolve copper(II) sulphate, or b) will coordinate to
the copper or otherwise form a crystalline solvate.
For copper(II) sulphate, esters, ketones and most alcohols simply won't dissolve the compound in the first place. Methanol might, but I wouldn't be
surprised if it crystallized with methanol where water would be in the hydrate.
Amines and nitriles will be more successful at dissolving the copper(II) sulphate, but they will coordinate the copper, and will remain part of the
crystal when it crystallizes. I'm not sure I'd even trust an amide.
A sulphate melt might work, but I think it's quite difficult to get things to precipitate from a melt, and you're also likely to form double salts
such as Na2Cu(SO4)2. (I wonder if choline sulphate would form a low temperature melt? Or a mixture of nitrate and sulphate?)
Something like DMSO might work, but then again, it might solvate.
Please remember: "Filtrate" is not a verb.
Write up your lab reports the way your instructor wants them, not the way your ex-instructor wants them.
|
|
aga
Forum Drunkard
Posts: 7030
Registered: 25-3-2014
Member Is Offline
|
|
It is dat you is kiddin' right ?
Grinning X to a Yard of X requires anhydrous conditions, so the challenge is to keep all water out or it dunt work properly.
Cl2 and Sulphur - Gas meets Solid, makes Liquid, and no water in sight ...
Trust me - reactions with S2Cl2/SCl2 are far from tedious !
Destroying the stuff then cleaning up the glassware is tedious, so maybe you got a good point there.
|
|
crystal grower
Hazard to Others
Posts: 474
Registered: 3-1-2016
Location: Os Petrosum
Member Is Offline
Mood: Puzzled
|
|
So I have found the article on my phone, I hope the link will work fine:
http://nvlpubs.nist.gov/nistpubs/jres/68A/jresv68An3p313_A1b...
Actually there isn't used only sulfuric acid but also ammonium sulfate is added to increase solubility of copper sulfate.
|
|
NEMO-Chemistry
International Hazard
Posts: 1559
Registered: 29-5-2016
Location: UK
Member Is Offline
Mood: No Mood
|
|
You mentioned fermentation, you have short weekly slots..............
How about a couple of different fermentations along the lines of:
# Yeast - Ethanol (distil after)
# ABE Fermentation with bacteria to get Acetone,Butanol and Ethanol (again you can distil)
# Making Citric acid via a fungus (A.Niger)
You should be able to show a range of Biochemical processes that dont need much looking after but should prove interesting. With 2 hour time slots you
dont want to be caught out time wise/
The above could be done at the same time and show a theme/thread, it should also prove to be pretty interesting and requires a variety of different
lab skills. The bacteria and moulds you should be able to pick up easily (ish).
There is probably other processes that are similar, All are or were industrial processes.
I havnt managed to do the Citric acid or the ABE one yet but they are on my to do soon list.
EDIT
Hang on i will see if i can post some papers to give you an idea what i am on about
[Edited on 14-9-2016 by NEMO-Chemistry]
Attachment: ABE2.pdf (2.7MB) This file has been downloaded 684 times
[Edited on 14-9-2016 by NEMO-Chemistry]
Attachment: citric acid production.pdf (395kB) This file has been downloaded 457 times
Let me know if you want more info, i collected some papers on these for when i get around to it. For straight Ethanol from yeast, you could compare
immobilized yeast and free yeast cultures.
[Edited on 14-9-2016 by NEMO-Chemistry]
Attachment: ImmobilisedYeast2.1_UK_eng.pdf (885kB) This file has been downloaded 1008 times
You should be able to get alot done over a year doing this, but it should also be doable within 2 hour slots.
[Edited on 14-9-2016 by NEMO-Chemistry]
Nearly forgot Acetic Acid as well! And all should be cheap to do and relatively simple.
[Edited on 14-9-2016 by NEMO-Chemistry]
Another immobilized yeast paper, i found it pretty interesting but your mileage may vary lol .
[Edited on 15-9-2016 by NEMO-Chemistry]
Attachment: imo yeast.pdf (735kB) This file has been downloaded 402 times
|
|
DraconicAcid
International Hazard
Posts: 4333
Registered: 1-2-2013
Location: The tiniest college campus ever....
Member Is Offline
Mood: Semi-victorious.
|
|
Interesting. I wonder if you could diffuse sulphuric acid into the mixture at a stable temperature to get crystals of anhydrous CuSO4.
Please remember: "Filtrate" is not a verb.
Write up your lab reports the way your instructor wants them, not the way your ex-instructor wants them.
|
|
Scalebar
Hazard to Self
Posts: 54
Registered: 6-5-2016
Location: Europe!
Member Is Offline
Mood: Looking for a way out
|
|
Physarum ( slime mold ) chemotaxis & other responses or its potential as a bio-oil producer if you do a solvent extraction on a bulk culture. I'd
even send you the physarum culture for nothing How could anyone not want a giant
maze solving amoeba?
|
|
NEMO-Chemistry
International Hazard
Posts: 1559
Registered: 29-5-2016
Location: UK
Member Is Offline
Mood: No Mood
|
|
Quote: Originally posted by Scalebar | Physarum ( slime mold ) chemotaxis & other responses or its potential as a bio-oil producer if you do a solvent extraction on a bulk culture. I'd
even send you the physarum culture for nothing How could anyone not want a giant
maze solving amoeba? |
I had to look that up! What a cool organism, what kind of things you doing with it?
This is way cool! Almost like some Alien life form
The Tokyo experiment paper
[Edited on 15-9-2016 by NEMO-Chemistry]
Attachment: Physarum.pdf (415kB) This file has been downloaded 425 times
|
|
Scalebar
Hazard to Self
Posts: 54
Registered: 6-5-2016
Location: Europe!
Member Is Offline
Mood: Looking for a way out
|
|
I use it for shooting time lapse movies ( you can find them on Youtube on the Oddscience channel ), messing around with mazes and doing science
outreach sessions for schools. In the lab I keep some on the go fed with fluorescence dyes for microscope testing.
I post the stuff out world wide as a dried culture free of charge - you can keep them alive on wet paper with a few oats as food. If you want some,
just shout.
|
|
NEMO-Chemistry
International Hazard
Posts: 1559
Registered: 29-5-2016
Location: UK
Member Is Offline
Mood: No Mood
|
|
Quote: Originally posted by Scalebar | I use it for shooting time lapse movies ( you can find them on Youtube on the Oddscience channel ), messing around with mazes and doing science
outreach sessions for schools. In the lab I keep some on the go fed with fluorescence dyes for microscope testing.
I post the stuff out world wide as a dried culture free of charge - you can keep them alive on wet paper with a few oats as food. If you want some,
just shout. |
Now that would be cool! I have spent days reading about them (hence my absence). Utterly amazing, i will shout you once i am happy i have enough info
.
|
|