Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Printable Version  
 Pages:  1  ..  30    32    34  ..  77
Author: Subject: Pretty Pictures (2)
alexleyenda
Hazard to Others
***




Posts: 277
Registered: 17-12-2013
Location: Québec, Canada
Member Is Offline

Mood: Busy studying chemistry at the University

[*] posted on 16-5-2015 at 10:36


Photos from my internship:

What the guy beside me do :


reac rouge mottons.jpg - 65kB

What i do while he sacrifices virgins :

reac flash.jpg - 51kB

-_-'




[Edited on 16-5-2015 by alexleyenda]




Help us build the Sciencemadness Wiki! Every question and tips about amateur chemistry two clicks away, wouldn't that be awesome?! sciencemadness.org/smwiki
View user's profile View All Posts By User
Zombie
Forum Hillbilly
*****




Posts: 1700
Registered: 13-1-2015
Location: Florida PanHandle
Member Is Offline

Mood: I just don't know...

[*] posted on 16-5-2015 at 12:49


It's a tough call as to who has the better job...



They tried to have me "put to sleep" so I came back to return the favor.
Zom.
View user's profile View All Posts By User
blogfast25
International Hazard
*****




Posts: 10562
Registered: 3-2-2008
Location: Neverland
Member Is Offline

Mood: No Mood

[*] posted on 16-5-2015 at 12:56


When fermenting berries in the lab, always strain the mash first!



View user's profile View All Posts By User
Zombie
Forum Hillbilly
*****




Posts: 1700
Registered: 13-1-2015
Location: Florida PanHandle
Member Is Offline

Mood: I just don't know...

[*] posted on 16-5-2015 at 13:15



Meme+00085.jpg - 166kB




They tried to have me "put to sleep" so I came back to return the favor.
Zom.
View user's profile View All Posts By User
alexleyenda
Hazard to Others
***




Posts: 277
Registered: 17-12-2013
Location: Québec, Canada
Member Is Offline

Mood: Busy studying chemistry at the University

[*] posted on 16-5-2015 at 13:27


^^By the way, the red stuff was a kind of Iron 2+ complex with a bidental triple cycle ligand, I forgot it's name, anyway it's not my project as I said :p




Help us build the Sciencemadness Wiki! Every question and tips about amateur chemistry two clicks away, wouldn't that be awesome?! sciencemadness.org/smwiki
View user's profile View All Posts By User
Texium
Administrator
********




Posts: 4618
Registered: 11-1-2014
Location: Salt Lake City
Member Is Offline

Mood: PhD candidate!

[*] posted on 16-5-2015 at 13:49


Quote: Originally posted by MrHomeScientist  
I've tried that one and it yields Bi powder, which isn't very interesting to me so I tried melting it down to an ingot. That failed, and instead it oxidized to yellow bismuth trioxide! Too finely powdered, I guess.
Yeah, I had the same experience! Even when I tried to melt it under argon (using a wine preservation canister). Oh well. It isn't very pretty for the element collection but at least it still works for chemistry.



Come check out the Official Sciencemadness Wiki
They're not really active right now, but here's my YouTube channel and my blog.
View user's profile Visit user's homepage View All Posts By User
Gleb
Harmless
*




Posts: 8
Registered: 23-4-2015
Location: Russia
Member Is Offline

Mood: No Mood

[*] posted on 17-5-2015 at 02:28
My collection (others)


1. Mn(SO4)2
2. naphthalene
3. thiourea
4. Na2B4O7
5. K2SO4*NiSO4
6. Bi


qGPQPiFTnNY.jpg - 30kBTgjSUZdWNr4.jpg - 67kB2wQYPkYCBvA.jpg - 26kByziUe21_G4o.jpg - 39kBOYEnhzkJh0M.jpg - 25kBsyDrkGbqgdM.jpg - 62kB
View user's profile View All Posts By User
smaerd
International Hazard
*****




Posts: 1262
Registered: 23-1-2010
Member Is Offline

Mood: hmm...

[*] posted on 17-5-2015 at 04:05


Nice flask there Alexleyenda. Love the column too. I learned a lot doing an internship like program hope you did too.



View user's profile View All Posts By User
Wizzard
Hazard to Others
***




Posts: 337
Registered: 22-3-2010
Member Is Offline

Mood: No Mood

[*] posted on 17-5-2015 at 08:16


Gleb - Beautiful work, there!! I aspire to grow my own as well as yours. Can you tell me anything about the potassium sulfate and nickel sulfate crystal in your last picture?

Nizzo - Nice Nd sulfate crystals! How do you prevent yours from cracking? My medium sized ones (about that size) like to split along planes.
View user's profile View All Posts By User
Brain&Force
Hazard to Lanthanides
*****




Posts: 1302
Registered: 13-11-2013
Location: UW-Madison
Member Is Offline

Mood: Incommensurately modulated

[*] posted on 17-5-2015 at 21:38


<img src=http://i.imgur.com/vGCOVMu.jpg width=800>
<img src=http://i.imgur.com/cCwBiC6.jpg width=800>

The same holmium citrate solution, in tube lighting and CFL respectively.




At the end of the day, simulating atoms doesn't beat working with the real things...
View user's profile View All Posts By User
Gleb
Harmless
*




Posts: 8
Registered: 23-4-2015
Location: Russia
Member Is Offline

Mood: No Mood

[*] posted on 18-5-2015 at 01:55


Wizzard, thank you!
I crystallized the stoichiometric amount of nickel sulfate solution and potassium:
NiSO4+K2SO4+6H2O=K2SO4*NiSO4*6H2O (blue-green crystals)

temperature=20 C
quite fine chemicals
isometric evaporation method
View user's profile View All Posts By User
Brain&Force
Hazard to Lanthanides
*****




Posts: 1302
Registered: 13-11-2013
Location: UW-Madison
Member Is Offline

Mood: Incommensurately modulated

[*] posted on 18-5-2015 at 20:05


<img src=http://i.imgur.com/By8k73e.jpg width=800>

Here's some of the holmium citrate solution I'm drying, under CFL light. The above pictures aren't very accurate, as there still was a bunch of particulate metal pieces that hadn't fully dissolved yet.

Here are the crystals that I've already made:

<img src=http://i.imgur.com/1gJSk0a.jpg width=800>




At the end of the day, simulating atoms doesn't beat working with the real things...
View user's profile View All Posts By User
The Volatile Chemist
International Hazard
*****




Posts: 1981
Registered: 22-3-2014
Location: 'Stil' in the lab...
Member Is Offline

Mood: Copious

[*] posted on 26-5-2015 at 12:40


Cool! Very small, too bad. How much holmium do you own?



View user's profile Visit user's homepage View All Posts By User
aga
Forum Drunkard
*****




Posts: 7030
Registered: 25-3-2014
Member Is Offline


[*] posted on 26-5-2015 at 12:48


And there was B&F saying he had no Lab ...



View user's profile View All Posts By User
greenlight
National Hazard
****




Posts: 754
Registered: 3-11-2014
Member Is Offline

Mood: Energetic

[*] posted on 28-5-2015 at 07:19


Probably has already been done but rhodamine B in water:

[Edited on 28-5-2015 by greenlight]

20150528_232919.jpg - 3MB

[Edited on 28-5-2015 by greenlight]

20150528_233157.jpg - 3MB
View user's profile View All Posts By User
PHILOU Zrealone
International Hazard
*****




Posts: 2893
Registered: 20-5-2002
Location: Brussel
Member Is Offline

Mood: Bis-diazo-dinitro-hydroquinonic

[*] posted on 28-5-2015 at 11:14


Quote: Originally posted by greenlight  
Probably has already been done but rhodamine B in water:

[Edited on 28-5-2015 by greenlight]



[Edited on 28-5-2015 by greenlight]

Looks similar to phenolphtalein cristals falling in NaOH solution :D




PH Z (PHILOU Zrealone)

"Physic is all what never works; Chemistry is all what stinks and explodes!"-"Life that deadly disease, sexually transmitted."(W.Allen)
View user's profile View All Posts By User
The Volatile Chemist
International Hazard
*****




Posts: 1981
Registered: 22-3-2014
Location: 'Stil' in the lab...
Member Is Offline

Mood: Copious

[*] posted on 31-5-2015 at 14:24


Yeah. But, heck, phenolphthalein crystals? I only've ever had solutions of it :/
Did you make the Rhodamine, or purchase it?




View user's profile Visit user's homepage View All Posts By User
greenlight
National Hazard
****




Posts: 754
Registered: 3-11-2014
Member Is Offline

Mood: Energetic

[*] posted on 31-5-2015 at 18:57


@ volatile chemist;
I purchased the Rhodamine online.
View user's profile View All Posts By User
greenlight
National Hazard
****




Posts: 754
Registered: 3-11-2014
Member Is Offline

Mood: Energetic

[*] posted on 3-6-2015 at 06:04


Again; may have already been posted but some nice coloured smoke compos:):

Screenshot_2015-06-03-17-22-24.png - 4.7MB Screenshot_2015-06-03-17-23-05.png - 4.1MB

[Edited on 3-6-2015 by greenlight]


Screenshot_2015-06-03-17-18-51.png - 4.1MB

[Edited on 3-6-2015 by greenlight]

[Edited on 3-6-2015 by greenlight]

Screenshot_2015-06-03-17-21-23.png - 3.7MB

[Edited on 3-6-2015 by greenlight]
View user's profile View All Posts By User
DutchChemistryBox
Hazard to Self
**




Posts: 74
Registered: 24-3-2013
Location: Strasbourg
Member Is Offline

Mood: No Mood

[*] posted on 3-6-2015 at 09:52


Quote: Originally posted by greenlight  
Again; may have already been posted but some nice coloured smoke compos:):



[Edited on 3-6-2015 by greenlight]




[Edited on 3-6-2015 by greenlight]

[Edited on 3-6-2015 by greenlight]



[Edited on 3-6-2015 by greenlight]


Wow beautiful!

Can you tell us something about your compositions?




View user's profile View All Posts By User
greenlight
National Hazard
****




Posts: 754
Registered: 3-11-2014
Member Is Offline

Mood: Energetic

[*] posted on 3-6-2015 at 19:20


They are 50:30:20 Powder dye/Potassium chlorate/Lactose powder.
50 grams each wrapped in paper and tightly taped

Top left = Blue dye Top right = Purple dye (Rhodamine B)
Middle = Yellow solvent dye
Bottom = 50:50 Blue/yellow
View user's profile View All Posts By User
The Volatile Chemist
International Hazard
*****




Posts: 1981
Registered: 22-3-2014
Location: 'Stil' in the lab...
Member Is Offline

Mood: Copious

[*] posted on 4-6-2015 at 12:20


Cool, they look nice! Very opaque.



View user's profile Visit user's homepage View All Posts By User
Texium
Administrator
********




Posts: 4618
Registered: 11-1-2014
Location: Salt Lake City
Member Is Offline

Mood: PhD candidate!

[*] posted on 4-6-2015 at 14:04


Quote: Originally posted by greenlight  
Top left = Blue dye Top right = Purple dye (Rhodamine B)
Middle = Yellow solvent dye
Bottom = 50:50 Blue/yellow
Could you elaborate more on what the blue and yellow dyes consist of?



Come check out the Official Sciencemadness Wiki
They're not really active right now, but here's my YouTube channel and my blog.
View user's profile Visit user's homepage View All Posts By User
Volanschemia
Hazard to Others
***




Posts: 340
Registered: 16-1-2015
Location: Victoria, Australia
Member Is Offline

Mood: Pretty much all of them!

[*] posted on 4-6-2015 at 16:24


Yes, please. I would like to know that as well. They look really nice!



"The chemists are a strange class of mortals, impelled by an almost insane impulse to seek their pleasures amid smoke and vapor, soot and flame, poisons and poverty; yet among all these evils I seem to live so sweetly that may I die if I were to change places with the Persian king" - Johann Joachim Becher, 1635 to 1682.
View user's profile View All Posts By User
alexleyenda
Hazard to Others
***




Posts: 277
Registered: 17-12-2013
Location: Québec, Canada
Member Is Offline

Mood: Busy studying chemistry at the University

[*] posted on 4-6-2015 at 18:46


Quote: Originally posted by TheAustralianScientist  
Yes, please. I would like to know that as well. They look really nice!

I agree !

Today, in my internship, I made a zipper reaction, that is the result of ethylenediamine deprotonated by NaH, it becomes a nice purple !


11329668_575540119255398_533268627_n.jpg - 83kB11304469_575540042588739_157542487_n.jpg - 55kB




Help us build the Sciencemadness Wiki! Every question and tips about amateur chemistry two clicks away, wouldn't that be awesome?! sciencemadness.org/smwiki
View user's profile View All Posts By User
 Pages:  1  ..  30    32    34  ..  77

  Go To Top