haydz
Harmless
Posts: 21
Registered: 1-3-2005
Location: New Zealand!
Member Is Offline
Mood: No Mood
|
|
Setting up a lab!
Hey guys,
Im going to setup a lab in my garage kitchen, im wondering what sort of things id need to have to make it safe, and all the apparatus - what i need
for home experiments and what i dont need ![:)](./images/smilies/smile.gif)
any help ![:)](./images/smilies/smile.gif)
edit: if this is in the wrong section can someone please move it?
[Edited on 3-3-2005 by haydz]
|
|
haydz
Harmless
Posts: 21
Registered: 1-3-2005
Location: New Zealand!
Member Is Offline
Mood: No Mood
|
|
Beaker glass, 100mL 1 $5.90
Bunsen burner 1 $26.30
Conical flask, 150mL glass (Labglass) 1 $5.75
Crucible tongs 1 $4.55
Eyedropper, glass, rubber teat, 150mm long 1 $1.20
Funnel, plastic, 60mm diameter 1 $2.00
Measuring cylinder, 100mL, polypropelene 1 $6.20
Tripod 1 $11.65
Tripod gauze mat 1 $3.80
Thermometer, red spirit, -10 to 110 deg 1 $6.60
Petrie dishes 90mm with lid 5 $2.80
Test tube stopper, 0 hole, 1 hole, 2 hole (fits flask) 1 $1.35
Litmus, blue, 20 strips per book 1 book $1.10
Litmus, red, 20 strips per book 1 book $1.10
Indicator strips book, pH 1-11 1 book $1.25
Total = $81.55
Spotting tiles, plastic, 12 depressions 1 $5.45
Hydrochloric acid 200ml $4.65
Ammonia solution 200ml $5.00
Magnesium ribbon 90cm $4.50
Extras = $19.60
this is what im going to order so far, have i missed anything? ignore the prices - but if anyones interested its NZ dollars
|
|
BromicAcid
International Hazard
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 3237
Registered: 13-7-2003
Location: Wisconsin
Member Is Offline
Mood: Rock n' Roll
|
|
What kinds of experiments do you want to do? What intrests you? This is usually the hardest question to answer when someone first gets into
chemistry but it's the most essential as to which direction your equiptment will go.
|
|
neutrino
International Hazard
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 1583
Registered: 20-8-2004
Location: USA
Member Is Offline
Mood: oscillating
|
|
I believe that there was already at least one thread on this around here somewhere, search for it.
Haydz: Those prices are atrocious. You <b>really</b> need to shop around.
|
|
rift valley
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 103
Registered: 24-7-2004
Location: NH
Member Is Offline
Mood: semiconducting
|
|
Quote: | Originally posted by BromicAcid
What kinds of experiments do you want to do? What intrests you? This is usually the hardest question to answer when someone first gets into
chemistry but it's the most essential as to which direction your equiptment will go. |
Very true, I started my home lab about eight months ago and really didnt know what chems to buy. I first bought pyro related chems like KNO3 etc.
I've found if you just read old threads you will find experiemts that interest you so buy the chems they require, keep doing this and before long
you obtain a nice little chemical inventory and dont have to buy so many chemicals anymore.
|
|
haydz
Harmless
Posts: 21
Registered: 1-3-2005
Location: New Zealand!
Member Is Offline
Mood: No Mood
|
|
Quote: | Originally posted by neutrino
I believe that there was already at least one thread on this around here somewhere, search for it.
Haydz: Those prices are atrocious. You <b>really</b> need to shop around. |
yeah but these are NZ dollars, are they still atrocious?
|
|
haydz
Harmless
Posts: 21
Registered: 1-3-2005
Location: New Zealand!
Member Is Offline
Mood: No Mood
|
|
Quote: | Originally posted by BromicAcid
What kinds of experiments do you want to do? What intrests you? This is usually the hardest question to answer when someone first gets into
chemistry but it's the most essential as to which direction your equiptment will go. |
Everything
|
|
Twospoons
International Hazard
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 1314
Registered: 26-7-2004
Location: Middle Earth
Member Is Offline
Mood: A trace of hope...
|
|
NZ $? Who is your source? Being a kiwi myself, I'd like to know.
|
|
haydz
Harmless
Posts: 21
Registered: 1-3-2005
Location: New Zealand!
Member Is Offline
Mood: No Mood
|
|
if u live in welly, I can get those items from my mate. are they expensive or are they about right?
|
|
neutrino
International Hazard
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 1583
Registered: 20-8-2004
Location: USA
Member Is Offline
Mood: oscillating
|
|
Quote: | Originally posted by haydz
yeah but these are NZ dollars, are they still atrocious? |
Yes, they are. For example, you pay $1 for a stopper. No good company will sell you rubber stoppers individually. Instead, you buy them by the pound
(around $4.50/lb).
|
|
tom haggen
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 488
Registered: 29-11-2003
Location: PNW
Member Is Offline
Mood: a better mood
|
|
Come to think of it, I'm going to be officially setting up a lab soon. Obviously I'm interested in energetic chemistry, and also Organic
Chemistry. I think I’m going to get a couple round bottom flasks, a nice condenser, a vacuum adapter, a separatory funnel, a claisen adapter, a
thermometer adapter, a magnetic stirrer hot plate combo, I already have a ring stand, some rings, and a clamp, Anyone think I'm missing anything
for building a nice organic chemistry set. Keep in mind I'm still a novice so I won't be caring out any syntheses that use chromatography
[Edited on 4-3-2005 by tom haggen]
[Edited on 4-3-2005 by tom haggen]
N/A
|
|
guaguanco
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 216
Registered: 26-11-2003
Member Is Offline
Mood: heterocyclic
|
|
Quote: | Originally posted by tom haggen
Anyone think I'm missing anything for building a nice organic chemistry set.
|
Yeah, Organic Chemicals. You'll find the really fun ones are very difficult to obtain nowadays.
|
|
tom haggen
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 488
Registered: 29-11-2003
Location: PNW
Member Is Offline
Mood: a better mood
|
|
What like THF?
N/A
|
|
neutrino
International Hazard
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 1583
Registered: 20-8-2004
Location: USA
Member Is Offline
Mood: oscillating
|
|
Do you have anything to connect your boiling flask to your condenser?
|
|
tom haggen
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 488
Registered: 29-11-2003
Location: PNW
Member Is Offline
Mood: a better mood
|
|
Probably I will get a y adapter for that job neutrino.
N/A
|
|
guaguanco
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 216
Registered: 26-11-2003
Member Is Offline
Mood: heterocyclic
|
|
I was thinking of things like ethyl acetoacetate, thiourea, nitromethane, chloroacetic acid. Versatile synthons.
[Edited on 4-3-2005 by guaguanco]
|
|
tom haggen
Hazard to Others
![*](images/xpblue/star.gif) ![*](images/xpblue/star.gif)
Posts: 488
Registered: 29-11-2003
Location: PNW
Member Is Offline
Mood: a better mood
|
|
Funny you should mention nitromethane. I have some in 30% concentration in model air plane fuel, and that is one of the things I plan in purifying.
N/A
|
|