arkoma
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First SUCCESSFUL steam distillation
Well, I tried and tried and tried to generate enough steam in an oil bath (I hava a HUGE fear of fires) but it just didna work. So I appropriated my
sisters teapot (shhhhhhb!!!!!) and used the gas side burner on the BBQ grill. I actually ended upwith a visible amount of basil oil w00t w00t!!
Steam adapter:
LOTS of PTFE tape
In the thermometer adapter/stillhead
FAIL steam generator
OMG, some drunk swiped my sisters tea kettle
slightly reamed out the whistler hole--hopefully she doesn't catch me (it still whistles)
Can't really see it, but there isa layer of sweet basil oil on top of the H2O
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
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violet sin
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Nice work man, I have been really wanting to get distilling with steam my self. What all do you have planned? The possibilities are many. I started
a big planter if mint just for this, saved a gallon bag of Orange blossoms, 1.5gal of lemon zest and have orange peels, grapefruit peels, access to
annise, basil, parsley and more. Not from stores, home grown.
Looks to be a lot of fun. Can't wait to get started, but in the meantime time, keep posting. I find this subject interesting
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hyfalcon
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I've got a 6 X 30' patch of lemon balm I've been wanting to do this to. I've obviously got to scale up for mine though.
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arkoma
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I've got some pine gathered up and also some Encelia Turns out there is an intertesting looking benzaldehyde in the encelia.
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
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Loptr
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Title: 5-Acetyl-2-methoxybenzaldehyde
CAS Registry Number: 531-99-7
Additional Names: 3-Acetyl-6-methoxybenzaldehyde
Molecular Formula: C10H10O3
Molecular Weight: 178.18
Percent Composition: C 67.41%, H 5.66%, O 26.94%
Literature References: A natural plant growth inhibitor found in the leaves of Encelia farinosa A. Gray, Compositae. Isoln and synthesis from
3-acetyl-6-methoxybenzonitrile: Gray, Bonner, J. Am. Chem. Soc. 70, 1249 (1948).
Properties: Needles from alcohol or ether, mp 144°. Sublimes without decomp. Emits fragrant odor on prolonged heating. Sol in hot water, warm ether,
alcohol, benzene, chloroform. Practically insol in cold water, 5% HCl, 5% NaOH, petr ether, carbon tetrachloride. Sol with orange color in concd
mineral acids.
Melting point: mp 144°
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hyfalcon
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I thing black walnut has a similar growth inhibiting substance in it.
http://www.wvu.edu/~agexten/hortcult/fruits/blkwalnt.htm
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aga
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Neat.
Kettle as a steam generator.
Wish i had thought of that !
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arkoma
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I tried using a canning jar with pipe soldered to lid in oil bath at first FAIL.
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
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