SAM4CH
Hazard to Others
Posts: 162
Registered: 16-7-2004
Location: TA
Member Is Offline
Mood: PERFECT
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Chlorate free Chloride!!
I got a platinized niobium anode and I tried to make perchlorate, I faced problem in removing chlorides from chlorate, I can reach 1% w/w chloride
content but it should be less than 0.05% w/w ... I made fractinal recrystalization and I can get 0.03% w/w but it is so difficult and I lose some
chlorate during the process, I'd like to get a new method to remove chloride less than 0.05%..
Note: I do not like to use AgNO3, Pb(NO3)2 to precipitate chlorides
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12AX7
Post Harlot
Posts: 4803
Registered: 8-3-2005
Location: oscillating
Member Is Offline
Mood: informative
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Why?
I made perchlorate with platinized titanium and probably as much as 5-10% chloride!
Anode life sucked, but that is hardly a surprise with ameteur plated titanium.
Tim
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