symboom
International Hazard
Posts: 1143
Registered: 11-11-2010
Location: Wrongplanet
Member Is Offline
Mood: Doing science while it is still legal since 2010
|
|
What elements have you isolated?
Not the best title i seen a project another user was working on making a list of chemicals made by the SM community
I have this list with the video showing elements being isolated chemically.
Hope this can be inspiring for others
Here is my tiny list
I have isolated 9 elements
Hydrogen
Oxygen
Chlorine
Bromine
Iodine
Zinc
Iron
Sodium
Sulfur
Carbon
List of elements users have made 28 in total
Aluminium
Bismuth
Boron
Bromine
Caesium
Calcium
Carbon
Chromium
Copper
Gallium
Hydrogen
Iodine
Iron
Lead
Mercury
Nitrogen
Nickel
Oxygen
Phosphorus
Potassium
Silicon
Sodium
Sulfur
Tin
Titanium
Uranium
Vanadium
Zinc
My references
Aluminium
https://m.youtube.com/watch?v=qkyPvhapxQs
Americium
Not isolated
Antimony
Not isolated
Argon
Not isolated
Arsenic
elementcollector1
http://www.sciencemadness.org/talk/viewthread.php?tid=25979
Barium
Not isolated
Beryllium
Not isolated
Bismuth
Nilered
https://m.youtube.com/watch?v=grpSfjUImUs
Boron
http://www.youtube.com/watch?v=0QBCyOrjR2o
Bromine
Dougs lab
https://m.youtube.com/watch?v=HuHceKvSHk0
Cadmium
Not isolated
Caesium
https://m.youtube.com/watch?v=rSJGwnERIVU
Calcium
https://m.youtube.com/watch?v=KGMKlsG9_1o
Carbon
https://m.youtube.com/watch?v=XGLuZhBWLrQ
Cerium
Not isolated
Chlorine
https://m.youtube.com/watch?v=OoS3q1C8zts
Chromium
https://m.youtube.com/watch?v=nEzH_499mTo
Cobalt
https://m.youtube.com/watch?v=ft-zjHP7tWg
Copper
OTC
Dysprosium
Not isolated
Erbium
Not isolated
Europium
Not isolated
Fluorine
Not isolated
Gadolinium
Not isolated
Gallium
https://m.youtube.com/watch?v=sUSjWfBBu2Y
Germanium
Not isolated
Gold
OTC
Hafnium
Not isolated
Helium
Not isolated
Holmium
Not isolated
Hydrogen
https://m.youtube.com/watch?v=Mv8Thq9rZ3Y
Indium
Not isolated
Iodine
https://m.youtube.com/watch?v=OoS3q1C8zts
Iridium
Not isolated
Iron
https://m.youtube.com/watch?v=DBBt7IhHOFQ
Krypton
Not isolated
Lanthanum
Not isolated
Lead
Not isolated
Lithium
Not isolated
Lutetium
Not isolated
Magnesium
Not isolated
Manganese
Not isolated
Mercury
https://m.youtube.com/watch?v=AzNnQ4O8BTY
Molybdenum
Not isolated
Neodymium
Not isolated
Neon
Not isolated
Nickel
By thermite
Niobium
Not isolated
Nitrogen
OTC
Osmium
Not isolated
Oxygen
https://m.youtube.com/watch?v=Mv8Thq9rZ3Y
Palladium
OTC
Phosphorus
https://m.youtube.com/watch?v=mhFyVDBmDVk
Platinum
OTC
Potassium
Nurdrage posted just need to add link
Praseodymium
Not isolated
Rhenium
Not isolated
Rhodium
Not isolated
Rubidium
Not isolated
Ruthenium
Not isolated
Samarium
Not isolated
Scandium
Not isolated
Selenium
Not isolated
Silicon
https://m.youtube.com/watch?v=pHWN6C4I664
Silver
OTC
Sodium
https://m.youtube.com/watch?v=jCrFFVVcPUI
Strontium
Not isolated
Sulfur
OTC
Tantalum
Not isolated
Tellurium
Not isolated
Terbium
Not isolated
Thallium
Not isolated
Thorium
Not isolated
Thulium
Not isolated
Tin
Single displacment with zinc
Titanium
Thermite
Tungsten
Not isolated
Uranium
https://m.youtube.com/watch?v=bl3NamzoFrM
Vanadium
https://m.youtube.com/watch?v=M7qGTtMF7bY
Xenon
Not isolated
Ytterbium
Not isolated
Yttrium
Not isolated
Zinc
https://m.youtube.com/watch?v=3X9c6epL7HQ
Zirconium
Not isolated
If i didn't delete the edited by it would get long..
[Edited on 19-5-2018 by symboom]
|
|
|
j_sum1
Administrator
Posts: 6320
Registered: 4-10-2014
Location: At home
Member Is Offline
Mood: Most of the ducks are in a row
|
|
Cool.
Did you look on the wiki to see if there are any others? I know for example that thorium has been done.
I am in the process of digesting some tool steel in HCl to extract vanadium. It will eventually be a video - and quite different from Tdep's efforts.
His was recovery of the products of a thermite that was done on a beach. Separation of sand and oxide is quite different from separating Fe and V in
solution.
|
|
|
crystal grower
Hazard to Others
Posts: 474
Registered: 3-1-2016
Location: Os Petrosum
Member Is Offline
Mood: Puzzled
|
|
I have an article describing two methods for Cobalt metal starting with CoCl2 if someone's interested.
http://pieceofscience.com/cobalt-metal-preparation/
I thought about trying ZrCl4+Mg to get the zirconium but not sure how well would it work, have anyone done it before?
[Edited on 19-5-2018 by crystal grower]
|
|
|
symboom
International Hazard
Posts: 1143
Registered: 11-11-2010
Location: Wrongplanet
Member Is Offline
Mood: Doing science while it is still legal since 2010
|
|
Acually i got half way there is alot of info
Going to add more later with an edit
Just wanted to let the idea flow
I wanted to add the ones who have isolated
And in the refrence of my post i was going to add links to the findings in a post and youtube videos of isolations with the username
A compitition of who can isolate the most elements.
[Edited on 19-5-2018 by symboom]
|
|
|
12thealchemist
Hazard to Others
Posts: 181
Registered: 1-1-2014
Location: The Isle of Albion
Member Is Offline
Mood: Rare and Earthy
|
|
Hydrogen - Iron and sulphuric acid
Lithium (if it counts) - batteries
Boron - from borax via boric acid and documented in many places https://www.youtube.com/watch?v=FAxqKQQ0wZU
Carbon - from thermal decomposition of sucrose
Oxygen - from thermal decomposition of potassium permanganate
Sodium - NaOH/Mg
Silicon - sand/Mg
Sulphur - sodium thiosulphate and hydrochloric acid, but not sure if this is worth documenting given its availability 
Chlorine - potassium permanganate and hydrochloric acid
Vanadium - from vanadinite mineral (far from perfect process - digest with HNO<sub>3</sub>, ppt Pb with NaCl, basify until
V<sub>2</sub>O<sub>5</sub> precipitated out, redissolved and reduced with zinc, ppt V(OH)<sub>3</sub>, thermally
decomposed, then thermite
Chromium - chromic oxide/Mg
Manganese - Mn<sub>2</sub>O<sub>3</sub>/Mg https://www.youtube.com/watch?v=3f6VE1USBDQ
Iron - Rust/Al
Cobalt - CoCl<sub>2</sub> displacement with Zn
Copper - displacement from copper sulphate solution https://www.youtube.com/watch?v=li0HmTZZuzw
Gallium - electrolysis of sodium gallate
Bromine - KBr/MnO<sub>2</sub>/sulphuric acid
Antimony - stibnite reduction with aluminium
Mercury - from cinnabar via Plante1996's process, documented by NileRed https://www.youtube.com/watch?v=0e78I9_oH1E&t=601s
|
|
|
symboom
International Hazard
Posts: 1143
Registered: 11-11-2010
Location: Wrongplanet
Member Is Offline
Mood: Doing science while it is still legal since 2010
|
|
Acually that was exactly i had in mand a lot more organized and detailed too
Yes extraction from batteries count
Just not strait out buying it pure
Edit removed my long signature
[Edited on 19-5-2018 by symboom]
|
|
|
Foeskes
Hazard to Others
Posts: 156
Registered: 25-2-2017
Member Is Offline
Mood: No Mood
|
|
I made cobalt with thermite before.
Crude and low quality manganese can also be made with MnO2 Thermite with excess Aluminium.
|
|
|
VSEPR_VOID
National Hazard
Posts: 719
Registered: 1-9-2017
Member Is Offline
Mood: Fullerenes
|
|
Make sure to add what you make to the SM list
https://docs.google.com/document/d/1AoI2VA5L4bmFw2HwXS2OVYTV...
Within cells interlinked
Within cells interlinked
Within cells interlinked
|
|
|
JJay
International Hazard
Posts: 3440
Registered: 15-10-2015
Member Is Offline
|
|
I'm more into collecting compounds than elements, so my list is pretty meager, but it includes bromine, hydrogen, oxygen, zinc, carbon, chlorine,
copper, and sulfur... probably a few more....
|
|
|
MrHomeScientist
International Hazard
Posts: 1806
Registered: 24-10-2010
Location: Flerovium
Member Is Offline
Mood: No Mood
|
|
I've done quite a few via Goldschmidt (thermite) reactions: B, Si, Ti, V, Cr, Mn, Fe, Sn
Elements isolated from other reactions: H, C, N, O, Cl, K, Cu, Br, Ag, I, Nd (maybe)
Plus a few more "isolated" from OTC sources, like Li from batteries, but I don't think that really counts.
Each has its own story, but would take quite a lot of time and space to write out!
|
|
|
woelen
Super Administrator
Posts: 8013
Registered: 20-8-2005
Location: Netherlands
Member Is Offline
Mood: interested
|
|
I isolated the following elements:
Br2 : NaBr + NaHSO4, using electrolysis
Cl2 : TCCA + HCl, Ca(OCl)2 + HCl, bleach + HCl
I2 : KI + dil. HCl + dil. H2O2
Se : Na2SeO3 + dil. HCl + SO2 (or sulfite)
P4: heating of red P
As : Reduction of As2O5 in conc. HCl, using SnCl2 (bad yield, just 10% or so, dared not use stronger reductant, because of fear of formation of AsH3)
C : heating of wood, sugar, starch
H2 : Zn + HCl, Mg + HCl
K : Mg + KOH + t-butanol in alkane solvent and heating
Ag : From AgNO3 and hydroquinone in solution, gives very fine powder
Cu : From CuSO4 and sodium dithionite in solution, gives very fine powder
S : From Na2S2O3 and dil. HCl
Of most elements, mentioned above, the making and isolation of them in a reasonable state of purity only is interesting for the sake of experimenting
and practicing certain types of chemistry. For me, the only elements worth isolating for having access to the element itself are Br2, Cl2, K, P4 and
As. The other elements I bought. This was easier and also cheaper than making them myself and gives me much better purity. The most succesful one for
me is bromine. I made a fairly large amount of that at high purity and perfectly dry and made a few nice samples of that. My powdered As-sample is
nice, but small, it only is 200 mg or so.
|
|
|
symboom
International Hazard
Posts: 1143
Registered: 11-11-2010
Location: Wrongplanet
Member Is Offline
Mood: Doing science while it is still legal since 2010
|
|
Here is the elements isolated by the comunity 32 elements
32 elements isolated
Out of 92 elements
We are 1/3 the way there
Someone double check this
Arsenic
Aluminium
Antimony
Bismuth
Boron
Bromine
Caesium
Calcium
Carbon
Chromium
Cobalt
Copper
Gallium
Hydrogen
Iodine
Iron
Lead
Manganese
Mercury
Nitrogen
Nickel
Oxygen
Phosphorus
Potassium
Silicon
Sodium
Sulfur
Silver
Selenium
Tin
Titanium
Uranium
Vanadium
Zinc
Excluding the very hazardous
21 total
Helium
Argon
Neon
Krypton
Xenon
Radon
Fluorine
Francium
Radium
Cadmium
Barium
Promethium
Thallium
Polonium
Astatine
Francium
Actinium
Protactinium
Fluorine
Technetium
Beryllium
39 elements left to isolate
Also started this thread so aga wont keep saying no one does any real chemistry on here and prove him wrong :/
So any ideas about a Hazard count by elements isolated
Using the least amount of reagents
[Edited on 23-5-2018 by symboom]
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
:
