morsagh
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Recrystallization problems
I prepared 9-phenylacridine, 1,4-diacridinobutane and 9-methylacridine but i have problem with recrystallizing them out of EtOH solution, because
everytime i get some liquid product. Don´t you know how to get crystals of acridine derivates?
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Ozone
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Although the translation is poor (the images are better), you may have better luck isolating them in salt form:
http://www.google.com/patents/US1629873
O3
[Edited on 8-3-2016 by Ozone]
-Anyone who never made a mistake never tried anything new.
--Albert Einstein
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Metacelsus
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In general, if a compound starts to come out of solution when the temperature is still above its melting point, you will get an oil instead of
crystals. You might want to try using a different solvent system.
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morsagh
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It is room temperature, i will try hydrochloric acid.
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