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Magpie
lab constructor
Posts: 5939
Registered: 1-11-2003
Location: USA
Member Is Offline
Mood: Chemistry: the subtle science.
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I would take a good look at the oil in your pump. It may need changing.
The single most important condition for a successful synthesis is good mixing - Nicodem
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Detonationology
Hazard to Others
Posts: 362
Registered: 5-5-2015
Location: Deep South
Member Is Offline
Mood: Electrophillic
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Damn, I had it open to clean some GAA residue just before I distilled!  Yay,
more practice!
“There are no differences but differences of degree between different degrees of difference and no difference.” ― William James
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