Hellbat
Harmless
Posts: 16
Registered: 23-2-2014
Member Is Offline
Mood: No Mood
|
|
NHN from hydrazine sulfate?
Hello,
is there a way to synthesize NHN (nickel hydrazine nitrate) directly from hydrazine sulfate without first making hydrazine hydrate?
I ask because I have quite some hydrazine sulfate lying around and I don't want to buy hydrazine hydrate.
Best regards
Hellbat
|
|
|
hissingnoise
International Hazard
Posts: 3940
Registered: 26-12-2002
Member Is Offline
Mood: Pulverulescent!
|
|
Use barium or calcium hydroxide to 'take out' the sulphate!
|
|
|
Hellbat
Harmless
Posts: 16
Registered: 23-2-2014
Member Is Offline
Mood: No Mood
|
|
But I wanted to go without forming hydrazine hydrate. When doing the classic hydroxide way, I think you won't get even close to 80%.
Also, the yield is very poor.
|
|
|
Amos
International Hazard
Posts: 1406
Registered: 25-3-2014
Location: Yes
Member Is Offline
Mood: No
|
|
So what if you used barium or calcium nitrate to precipitate the insoluble sulfate and get hyrazine nitrate? This thread might be useful: http://www.sciencemadness.org/talk/viewthread.php?tid=874
|
|
|
Hellbat
Harmless
Posts: 16
Registered: 23-2-2014
Member Is Offline
Mood: No Mood
|
|
And that would help me making NHN?
|
|
|
hissingnoise
International Hazard
Posts: 3940
Registered: 26-12-2002
Member Is Offline
Mood: Pulverulescent!
|
|
You really should have some understanding of the processes involved before attempting to produce this potent primary?
Read up on it, rather than persist with these beginner questions!
|
|
|
Hellbat
Harmless
Posts: 16
Registered: 23-2-2014
Member Is Offline
Mood: No Mood
|
|
Don't understand me the wrong way, I have quite some experience with explosives and chemistry in general.
I just asked for a full synthesis with hydrazine nitrate.
|
|
|
Bert
|
Thread Moved
10-1-2015 at 13:02 |
![[*]](images/xpblue/default_icon.gif){kind=icon}
