kmno4
International Hazard
Posts: 1497
Registered: 1-6-2005
Location: Silly, stupid country
Member Is Offline
Mood: No Mood
|
|
diphenyl oxalate - an attempt....
Post temporarily removed.
All thanks or complains please send to our local clown Bfesser.
[Edited on 21-2-2014 by kmno4]
Слава Україні !
Героям слава !
|
|
|
Marvin
National Hazard
Posts: 995
Registered: 13-10-2002
Member Is Offline
Mood: No Mood
|
|
Much respect for trying this but please don't taste an experimental compound ever again.
Fingers crossed it is the ester.
|
|
|
Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
This is very interesting! I remember reading some papers in which dimethyl oxalate is used with a Ti catalyst and phenol to produce the target
compound. Might be another route to experiment with since dimethyl oxalate is so easy to prepare?
http://www.orgsyn.org/demo.aspx?prep=cv2p0414
http://www.paper.edu.cn/selfs/downpaper/wangshengping286217-...
|
|
|
Marvin
National Hazard
Posts: 995
Registered: 13-10-2002
Member Is Offline
Mood: No Mood
|
|
Second paper isn't working for me, it goes directly to the site front page. Can you attach it?
That was the method I was going to try, but I didn't know about the catalyst. I was also thinking about transesterification.
|
|
|
Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
Sure thing, no clue why that happened...
Attachment: DPO via Transesterification.pdf (109kB)
This file has been downloaded 1152 times
|
|
|
bfesser
|
Thread Moved
21-2-2014 at 09:57 |
![[*]](images/xpblue/default_icon.gif){kind=icon}
