jcm4679
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huang minlon reduction
hey. can anyone help me out with something? after preforming a huang-minlon modification of the wolff-kishner reduction how do you go about separating
the hydrazine hydrate, potassium hydroxide, and diethylene glycol from your product after the reaction takes place?? any help at all would really be
appreciated.
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ScienceSquirrel
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Dump the lot in ice water, extract with solvent.
Concentrate and distil or crystallise as appropriate.
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hankxmen
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would you be able to expand on other procedures/seperations on this reduction?
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arsphenamine
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The Huang-Minlon modification is covered in Wikipedia and mentions a refereed procedure in Organic Syntheses, Coll. Vol. 4, p.510 (1963).
A search on the latter should give you the information you need.
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hankxmen
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thanks!!! got it to work so helpful
[Edited on 27-2-2013 by hankxmen]
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Nicodem
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Thread Moved
27-2-2013 at 07:22 |
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