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Author: Subject: aluminum hydride?
soma
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[*] posted on 12-8-2011 at 17:59
aluminum hydride?


I had read that by adding P205 to a LAH reduction of a secondary amide, that aluminum hydride is formed and that it causes the reaction to happen much quicker (1/2 hr.) at room temperature, (as compared to 18 hrs. at 110C).

Anyone tried this?

(I'll try and dig up the reference.)
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