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Author: Subject: Sodium silicate synthesis from Cab-O-Sil? Or pure small mesh silica?
deadrush
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[*] posted on 14-8-2024 at 16:10
Sodium silicate synthesis from Cab-O-Sil? Or pure small mesh silica?


I tried both and honestly I didn't get the best results. I've made gallons of sodium silicate from the kittie litter silica gel with the blue mixed in. I was anticipating superior results. If it matters I use a 2:3:5 ratio, naoh, sio2, h2o.

As an aside....
So I've had good results by starting with a solventless reaction between the silica gel powder and naoh when mixed vigorously. I'll even heat the mix. It's quite exothermic even prior to h2o. This, I've found, results in less water required, less time heating and a more viscous, concentrated product.
HOWEVER, when I tried this same technique with the other 2 silica sources, the results weren't great.
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[*] posted on 14-8-2024 at 17:48


I like to use oil sweeping compound, and got the same results. After trying more hydroxide, everything started going into solution.

A little reading shows that cat litter is designed to be hydrophilic and the sweeping compound hydrophobic. I credited that to the slow reaction.





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