njl
National Hazard
Posts: 609
Registered: 26-11-2019
Location: under the sycamore tree
Member Is Offline
Mood: ambivalent
|
|
Chlorination
In Shulgin's report on the chlorination of 2C-H to 2C-C, he uses liquid chlorine as a reagent. Why can't chlorine gas just be bubbled through a
solution of 2C-C in a suitable solvent?
|
|
|
mackolol
Hazard to Others
Posts: 459
Registered: 26-10-2017
Member Is Offline
Mood: Funky
|
|
And who said it can't?
|
|
|
Antigua
Hazard to Others
Posts: 155
Registered: 27-9-2020
Member Is Offline
|
|
Bubbling a stoichiometric amount of gas in is very difficult. Maybe with a help of air pump it would be easier, but he had access to dry ice and
acetone, so why would he need to bother with some gas generators? It probably will work as long as suitable reaction conditions are employed.
|
|
|
mackolol
Hazard to Others
Posts: 459
Registered: 26-10-2017
Member Is Offline
Mood: Funky
|
|
I don't really think, that slight excess would do bad in this case. At least with 2C-B overbromination doesn't readily ocurr.
[Edited on 10-1-2021 by mackolol]
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
