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Author: Subject: My 2 neck flask is broken :(
vmelkon
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[*] posted on 18-11-2018 at 09:45
My 2 neck flask is broken :(


I was trying to distill some impure H2SO4 and this requires high temperature, even when I reduced the pressure to 13 cm mercury.

It was a 2 neck flask.
I had placed a solid glass stopper in one of the necks. I guess it expanded and cracked the neck :(

My glassware is broken and my heart is broken :(




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Ubya
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[*] posted on 18-11-2018 at 09:50


i would be scared more of the hot boiling sulphuric acid spilling than sad for the lost of a flask




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nimgoldman
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[*] posted on 18-11-2018 at 11:55


I feel for you.

I have melted one 3-neck flask when drying molecular sieves under vacuum using a heating mantle.

After several pieces of broken glassware, I think about purchasing the cheaper kinds (flasks, beaker) in quantity as they have limited life expectancy in every lab.
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VSEPR_VOID
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[*] posted on 18-11-2018 at 16:08


Press F to pay respects to the flask



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Dragonjack12
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[*] posted on 3-12-2018 at 12:06


F



Jack place
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[*] posted on 3-12-2018 at 12:30


https://www.youtube.com/watch?v=D05AB8xs7qA
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morganbw
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[*] posted on 3-12-2018 at 12:46


I basically love my glassware but life has chosen to show me that it can be broken. Start some lab work that requires this/a certain piece and the damn thing is sure to break. I just figured it was me and my karma.

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