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Author: Subject: What size beads to use in a Hempel column?
Sauron
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[*] posted on 29-4-2008 at 08:14


My buddy in the Bay Area who is in the bead business tells me that a Kg of 4mm OD 4mm long glass beads is $150 there, but that if I go root around at the Chatuchak weekend market I can find same for about $15. (Here = Bangkok).

I think I will wait till his next visit and let him go to the Market, as it is a hot crowded maze which I detest. I'd rather pay $150 than have to spend an hour or two there.




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S.C. Wack
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[*] posted on 29-4-2008 at 14:55


Two minutes of Google searching = $38.25 kilo (OK, 8 kg volume discount, firemountaingems.com). Include Matsuno with the other two Japanese companies that I named. The point is that with searching comes better things.

Someone is making nice ceramic ones in 3mm and 4x6 (getting close to the pony bead range), though I'm not sure if these are glazed well enough for this use. They are sold as "Greek".




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[*] posted on 29-4-2008 at 17:43


Is glass wool too dense to be used in a condenser?
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MagicJigPipe
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[*] posted on 30-4-2008 at 02:16


I've seen glass wool used to support packing material in tubes/condensers that weren't designed to be columns (ie no supports/indentations).

I'm not sure exactly how it would affect performance, though.




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Sauron
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[*] posted on 30-4-2008 at 20:29


The cheap Indian-made glass beads sold here for about $15 a Kg are definitely glass, and available in clear colorless form.

So there is no issue of glazed vs unglazed as there is with ceramic beads.

I noticed also that Aldrich sells PTFE Raschig rings as small as 3 mm x 3mm x 1 mm in a pack of 500. In (borosilicate glass they just resell Ace's product and smallest is 5 x 5 x 1 mm.

I shudder to think of Aldrich's pricing however.




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[*] posted on 11-6-2008 at 00:35


We looked into clear glass beads at the Chatuchak weekend market and came up empty. They had plenty of colored glass beads, but I wanted clear, and for that all they had was crystal (quartz) for about $300 a Kg.

So no dice.

Meanwhile I found a local source for PTFE tubing, wall thicknesses of 0.5 and 1 mm, ODs from 2 mm to 22 mm. They also have other fluoropolyner tubing and they do custom fabrication so I am asking for a quote for the following:

3 x 3 x 0.5 mm, qty 5000 pcs
4 x 4 x 0.5 mm, same qty
5 x 5 x 0.5 mm qty 3000 pcs
6 x 6 x 0.5 mm qty 3000 pcs

I already know what Aldrich sells the 3 mm and 6 mm PTFE raschig rings for in packs of 500 and 300 respectively.

The little rings are great for smaller columns up to 19mm ID and the larger for columns up to 30mm ID.

Hopefully the low local labor content will allow some economy because Aldrich is just too damned expensive.

For glass tubing, a small benchtop diamond cutoff saw, say 4" blade, selling for $100 or so in USA, from jewelers supplies is ideal for fast and easy parting of small diameter glass tubing. A stop can be added for repetitive parting to predetermined length. Feeding of stock is by hand and cooling is by water (a little messy.) This is another option if you don't mind spending some tedious hours making your own raschig rings.




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[*] posted on 11-6-2008 at 07:34


One more alternative is, assuming you have the equipment, to make packing from lengths of flint glass tubing. You will need a cutoff wheel, and these can be gotten from lapidary supply as "trim saws". There are various designs.. some are more suited to this than others.

Yes, its expensive, but the equipment will pay for itself, long term I think. Especially if you are fabbing your own glassware and cutting short lengths of tubing a lot.

Plus, you will have a way to cut up small rocks and crystals :)
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[*] posted on 11-6-2008 at 08:49


The following pretty much renders DIY moot, at least for me.

Chemglass sells 6mm berl saddler for $25/200 cc abd slightly more than $100 a liter.

The piece count is approx 250 to 200 cc and 1250 to the liter.

That is pretty damned cheap and the ceramic saddles are better packing than raschig tings.

The catalog number is CG-1284.

[Edited on 12-6-2008 by Sauron]




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