Quote: Originally posted by wg48temp |
Say you are gravity filtering a liquid and the initial depth of the liquid is 100mm with only a few mm of precipitate. The filtering rate is
approximately inversely proportional to the pressure differential across the filter and filter cake. So for a water solution 100mm deep that is a
differential pressure of 10mbar (10m=1bar) or an average of 5mbar. Lets assume it takes 20 minutes to filter.
|
Vacuum filtration does not work that way. Maybe changing the vacuum from 380 psi down to 190 psi would double the speed in some cases, but the speed
of flow is simply related to the difference between the ambient pressure and the vacuum in the filter flask. So there is little difference between
10 and 20 psi in most cases. And as mentioned, once you get to the vapor pressure of the solvent, it will boil, and little if any increase in speed
will occur.
If you have a tough filtration, the key is to use a larger diameter filter, so that you get more flow. Changing the vacuum can't do much, as it can
NEVER be over 1 atm of difference. You can also pressurized the input, which can allow much higher pressure differentials than 1 atm. But that
takes special equipment.
|