Hope it's a big room with a fume hood-
Please take your lab sample of nitro and NC to a safe place now. Spread them thinly on a large sheet of cardboard, light a down wind edge and burn
them. Take your phone or a friend's phone and video the burn- Post it to youtube and PM me the link. You may make more later, perhaps. But not until
you have learned some theory, a student lab is pointless without theory- And notes.
Go look at the sections on nitrocellulose and smokeless powder manufacture in Tenney Davis' Chemistry of Powder and Explosives- see what is done
commercially to stabilize nitrocellulose.
Ask some more questions after you have found answers to the below:
Look for the solubility information for different solvents and NC of different degrees of nitration. Think about why your NC behaved as it did on
trying to dissolve it?
Then look for a chemical BESIDES the bases- carbonates, ammonia, etc. that could be put into the later (2nd) boiling water bath to help desorb acid
residue from the fibers and ensure a longer stability. Come back with a name.
Then ask some more questions based on these readings. Write the questions carefully, well enough so someone who doesn't know much of what you do will
understand, without assuming anything. Go over what you write, think of how to say the most with the fewest words. Spell check it when finished.
This is your homework for the week- If you don't do the homework, you will not get to go on to the next class.
Class dismissed!
[Edited on 22-3-2014 by Bert] |