Hi
English is poor
What else I need to add in terms of security?
For Safety protective goggles , gloves , Runaway nitration for 2 litre cold water )
1) Nitration mixture cooled in the fridge (temperature: - or 0C .. 2 hours cooled)
2) Beaker the ice bath and Pentaerythritol it each time be scored as 1gram ( temperature temperature 5-7 degrees will not be allowed to rise )
3) Last Pentaeritritol is adding . 10 minutes later Nitration mixture hot water bath put 25 minutes After 25 minutes, poured into cold water ( hot
water bath 45 C )
4) Petn crystals wash with clear water . %1 sodium bicarbonate solition wash with petn crystals ( natural pH 7 pH is measured with pH paper )
5) PETN and Acetone is put in a glass container heated 50C ( hot water bath ) . PETN is After dissolving - PETN and acetone mixture poured cold water
> crystals appeared )
6) PETN is filtered . PETN wash with water >>> Drying hissingnoise - 6-9-2012 at 04:53
There's a long thread on PETN, here! Peroksit - 6-9-2012 at 04:57