today i trty to make titanium silicide , the reaction product are fine to use. so i take a consentred solution of TiCl3 in glass test tube and a HF
generator on anoter test tube (i know, the glass become H2SiF6) so i active the hf generator and bublet it with poly tube in the TiCl3 solution ,
imediatly a grayish white precipitate formed , after testing this mater correspond to the broer description of titanium silicide my question is at
wath temperature the H2SiF6 become gas and if i take a steel HF generator and a plastic test tube , does it will precipitate TiF3 (the TiF3 is
insolube in water). |