I'm experimenting with some soft polymer mixtures. Composites containing suspensions of carbon nano-tubes and fine metallic powders.
I need to extrude some short pieces (25 - 75mm maybe) about the thickness of dry spaghetti (1 - 2mm).
These part-cured mixtures have a consistency and malleability similar to a soft alkali metal, and it occurred to be that something like a sodium press
might be ideal (I've already ruined my wife's expensive Williams Sonoma garlic press: she doesn't know yet
I guess SPS systems are resigning solvent stills to the history books and I was wondering if anyone on the forum had one they are looking to get rid
of.
Also happy to hear DIY ideas but I haven't got an elaborate work bench or tools. Honestly, even something like this is going to be hard for me to
fabricate although it looks like a good design: http://pubs.acs.org/doi/abs/10.1021/ed004p918
Would rather buy an old one with a 1mm or 2mm die, even if it is on it's last legs.
Let me know inline or as a U2U. Have a small budget for this.
[Edited on 6-2-2011 by paulr1234]unionised - 6-2-2011 at 02:11
I once made some indium wire with part of an old preparative scale HPLC column, a length of brass rod and a bench mounted vice.
Because indium isn't that soft I had to heat the system a bit.
I had the bits lying around so a budget wasn't the issue. It did take some time sawing the end off the column.peach - 22-6-2011 at 18:03
A guy on eBay was selling little discs with EDM drilled holes in them for ooooo I dunno, a year? I didn't see a single one of them sell. They'd
probably have gone in the end of those presses well, and now they've disappeared. But it wouldn't be harder to drill a similar hole with a fine drill
bit.
Not sure how well that aluminium would hold up, but there also seems to be a stainless clay extruder from makin's which costs $49.95.
The PieceMaker (137 euro) thing looks like this inside;
[Edited on 23-6-2011 by peach]plastics - 28-6-2011 at 07:46
I have the stainless steel version of the Makin clay extruder and it can sure make some pretty sodium wire
peach - 28-6-2011 at 07:55
Brilliant!
Is it hard to get through the standard caps and does it feel like it stressing the extruder at all?
I'll probably pick one up if it's all okay with sodium.plastics - 28-6-2011 at 08:07
Peach - I haven't filled the whole thing up. Just used individual 1cm3 blocks to make some wire to dry up a bit of diethyl ether. Didn't seem to blink
at these
I will try it on a small block of lithium in the next few days to make some lithium bronze. Wacking a lump with a hammer and then cutting the sheet
into strips and then tiny squares is a right PITA
Cleaning it up at the end was interesting
Sodium wire
science4u - 4-7-2011 at 22:23
Hi there
I also need to make sodium wires...Please tell me your experience with the presses mentioned.
Rgds
peach - 5-7-2011 at 00:00
He just did didn't he, up there^ science4u - 5-7-2011 at 04:09
I dont know if you used the cheapest (20USD) or the other.
Someone used sodium? isnt it dangerous to work with sodium and with these presses?
Rgdspeach - 5-7-2011 at 09:26
He is using the second one, the Makin stainless steel clay extruder. Which is about $50.
Provided the press is dry and isn't dunked in water, the only thing that should happen is that the surface of the sodium will begin to oxidise.
Pushing it through the nozzle scrapes the surface clean just before it's dropped into some solvent that needs drying.
Using sodium wire like this is normal for drying solvents as much as is possible. Although universities are switching to a newer method as the sodium
+ solvent + heat presents a significant fire risk to staff and students; particularly those who aren't all that used to dealing with boiling,
flammable things.