Originally posted by UncleJoe1985
Hi everyone. I recently got into major trouble for doing chemical experiments in my dorm and am seeking advice on defending myself. I was
experimenting and improving nitric acid production using an arc furnace along with electrolytic production of chlorates and perchlorates for rocket fuel.
Actually, I was told to dismantle my equipment and safely remove all hazardous chemicals by the housing department a week before any major trouble
began. I dismantled my arc furnace, but didn't remove my chemicals because I wanted to find out which were allowed and which weren't because the
housing policy just said no hazardous chemicals, with a short list of flammables like lighter fluid. Unfortunately, instead of meeting with the
building manager to discuss the matter, an environment health services worker came too and said they had to remove everything for safe keeping.
Luckily, everything was labeled and they had no problem identifying anything and no laws were broken. They kept asking where I got the oxidizers and
nitric acid, which I said I made them, to which the EHS guy said he was very impressed. I admit I got argumentive, due to being unfairly accused of
planning to harming others and argued the amounts I were using/manufacturing were small.
Here's a list of chemicals they reported (amounts are from me - I don't think they bothered with the amounts):
30% nitric acid (~250 mL in beer bottle)
5 pounds sulfur (Rubbermaid container)
~300g ammonium nitrate (Rubbermaid container)
~3 Kg KClO3 (2L soda bottle)
~2 Kg NaClO3 (2L soda bottle)
~0.5 kg aluminum powder (Rubbermaid container) along with ball mill
~0.4 kg lead nitrate formed by dissolving lead fishing weights in nitric acid
~300 mL red cabbage indicator
~1.5 kg KCL ice melt
~4 L NaCl, NaClO, NaClO3 electrolyte solution
The next day, I was told I was temporarily suspended from the university and housing. I was also visited by 3 plainclothes FBI agents, who said they
were trying to determine if any explosives were made and if they had gotten out of the dorm. They were friendly at first, saying it's fun to play with
explosives, but not in a dorm. They seemed convinced that I was manufacturing explosives based on my Internet history and a bottle of unused H2O2 and
encouraged me to confess, which I definitely denied and said was for making Tin (IV) oxide for PbO2 anodes. Unfortunately, I made the mistake of also
denying knowledge of their manufacture, which made them frustrated. Eventually, I did recall looking up on the manufacture of HTMD, which seemed to
satisfy them and they left, taking a box of containers used in my experiments. Yesterday, I found out I will be able to go back on campus and finish
the semester, but will be suspended for the Spring.
I know I made a serious mistake in doing my experiments in my dorm, but I didn't expect it to be this serious. The main charge is for endangering
others and having unauthorized chemicals, but I think the severity is in question.
For example, I clearly stated in an apology/reflection letter that I stored all oxidizers away from any fuels, so to the best of my knowledge, nothing
would spontaneously combust (the KClO3 was in the same cabinet as the sulfur, aluminum powder, and ammonium nitrate, so that's probably already
contrary to how they store oxidizers in a lab. I also stated I never made any explosives.
Secondly, I asked them if the charge of harming others is based on potential harm or actual harm, and they said potential. Actual harm is not
debatable, but I don't know who they listened to for deciding potential harm. I read some MSDS sheets on the chemicals I used, and their hazard
ratings were a lot higher than I expected. It seems that the hazards are based on the danger to the absolute most careless person (not including
children) and the worst possible case. For example, the MSDS for NaCl says it's hazardous: warning - may cause eye irritation. Honestly, who puts salt
in their eyes? I wouldn't be surprised if water had a MSDS saying it might cause drowning. I'm not saying this in jest because reality is based on
perception and is different for everyone.
I have the option to appeal, but haven't decided if there's reason to. Any comments or suggestions?
[Edited on 27-11-2008 by UncleJoe1985] |