Sciencemadness Discussion Board

Tour My Lab

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Magpie - 19-11-2013 at 18:39

Quote: Originally posted by MrHomeScientist  

I'm trying to figure out my own fume hood situation - the problem at the heart of it all is where do the fumes exit the house. It's looking like either cut a hole in my roof (which I really do not want to do) or go up into my attic, make a U-turn, and come out the soffit. I know sharp turns are bad for airflow, but it's what I'm forced to do in the current location (garage wall).


Can you install a louvered outlet in the peak of your attic? If so, mount the blower just inside that peak. A squirrel cage blower will make the 90° turn for you.

MrHomeScientist - 20-11-2013 at 12:36

Magpie: Do you mean an outlet in the side of the house (facing the street), instead of putting one in the roof? Like this:

That's an excellent idea. That way I don't have to punch a hole in the roof using my godawful carpentry skills, nor would I have to have an unsightly pipe sticking out above my garage. This would also give me more room to gently bend the pipe and not have to maneuver around sharp turns.

The problem then becomes that I would probably need to keep the garage door closed when working, so fumes don't drift down and back into the work area. It'll get hot out there in the summer!

Magpie - 20-11-2013 at 13:56

Yes, that looks like a bisected grate in that peak. It would be better if the grate were located a foot or two lower so that it would mate up better with the blower outlet.

Yes, you can't leave your garage door open when using the blower, other wise you would be "eating your own dirt," so to speak. I leave the garage door open to my living quarters then go to the other end of the house and open a bedroom window. This draws fresh air into the garage that passes through the whole house. And yes you pay a heating or cooling price for using that conditioned air. Nobody said safety was cheap.

violet sin - 21-11-2013 at 03:47

if it goes up through your attic, make sure you consider safety first. perhaps a good air duct (rolled sheet metal kind) if there is a chance of sucking up flames from a broken piece of glassware. you really don't wanna have a problem with flame, some of the cheap dryer vent flex tube and forced air. especially in an open beam part of the structure you live in. you should really check with local standards first and foremost.

I installed 2 vent fans for a glass blowers studio, both 12" inline exhaust fans. One under the eve near the peak, the other was through a window I pulled out. we kept the eave vent intake well away from all heat sources. the window one behind the torch was set in concrete board and had no ducting behind it to burn out. we observed all safety requirements and it got plenty of use safely.

MrHomeScientist - 21-11-2013 at 13:08

Thanks, Magpie. This option is definitely something to think about.

violet sin, I don''t think flexible dryer tubing is suitable for a fume hood line. They are made from thin aluminum, which would quickly corrode if any acid fumes are passed through them. My thought was to use PVC piping. This probably isn't great for solvent vapors, but hopefully stands up well enough to last (plus I don't generally use organic solvents). If it does get eaten up I can easily pop in a new segment.

[Edited on 11-21-2013 by MrHomeScientist]

violet sin - 22-11-2013 at 01:09

I was just pointing that out. the flex tube is not a good idea, though its commonly used for bathroom vent/light combo fans. and it would surely be recommended by a home improvement store employee if you gave him scant details on what exactly you were doing. so thought I would bring it up.

MrHomeScientist - 22-11-2013 at 07:26

Apologies, I must have misread your post. I get a lot of weird looks when I try to describe my construction projects to hardware store employees, for sure.

Steve_hi - 24-11-2013 at 16:22


Hi we just recently finished our fume hood and so we are posting pictures.

C:\Users\steve\Desktop\fumehood\november 011.jpg

[img]C:\Users\steve\Desktop\fumehood\today saturday 009.jpg[/img]

[img]C:\Users\steve\Desktop\fumehood\today saturday 010.jpg[/img]

[img]C:\Users\steve\Desktop\fumehood\today saturday 011.jpg[/img]

[img]httpC:\Users\steve\Desktop\fumehood\today saturday 012.jpg://[/img]

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UnintentionalChaos - 24-11-2013 at 17:13

Quote: Originally posted by Steve_hi  

Hi we just recently finished our fume hood and so we are posting pictures.


That is a gorgeous workspace! I am also jealous of that vacuum pump. I have the single stage version that pulls 30torr and would love the versatility of the two-stage.

prof_genius - 25-11-2013 at 09:12

Quote: Originally posted by Steve_hi  

Hi we just recently finished our fume hood and so we are posting pictures.



Looks great, I like how you personalized it with the photos. :)

Hexavalent - 2-12-2013 at 12:43

Comments and queries are welcome. :P

http://s1032.photobucket.com/user/joeanderson98/slideshow/

ScienceHideout - 2-12-2013 at 18:36

Quote: Originally posted by Hexavalent  
Comments and queries are welcome. :P

http://s1032.photobucket.com/user/joeanderson98/slideshow/


WAAY to clean for me to work in :P

Lol, I am messy :( What is your secret to being organized?

Pyro - 3-12-2013 at 07:42

Mine is to have a little OCD. Stealing cabinets is very relaxing, like meditation and it allows you to put stuff under lock and key.

SH, can you give us a tour of your lab please?

ScienceHideout - 5-12-2013 at 16:48

Sure, Pyro. I will one day. It is rather impressive. I would just like to get it looking presentable first. I know that no one will judge me on how neat it is, but I need to clean it anyways, so this is a good excuse :)

Pyro - 5-12-2013 at 16:52

well then, PICS! :) I am always curious to see other peoples labs to be able to look at alongside of mine so I can see what I forgot.
I would post yet another lab tour since yet more things have been changed, but I think people here are sick of me posting a tour every time I make a change :(

Zephyr - 22-1-2014 at 17:18

Here is my lab;




Some glassware;




And my element collection (I have many gases including Br, Cl, He, but the ampoules don't fit in my home made case).


cyanureeves - 22-1-2014 at 18:45

nice one pinkhippo.i have been thinking for a long time that the key to a clean lab is to have white walls and if possible floors.if i ever get a chance to build a lab i will first paint everything white acrylic latex or shiny oil base white.it is easier to find spots and splatters and small items in a clean white room.

Zephyr - 22-1-2014 at 18:52

Thank you and yes, it does make it easy to clean, although the floor and lower portions of my walls are cement. The downside of white walls is that once you get a little bit of a dye, like Fluorescein on them, it gets every where and when you try to wipe it up, it just spreads further.

confused - 23-1-2014 at 00:32

Im envious of you guys with dedicated lab space :P

alexleyenda - 23-1-2014 at 00:33

Wow the labs posted in the 2 last pages are awesome, I look forward to making money after my studies and not have anymore to plug my distillation apparatus in a 2m² bathroom on a chair and experiment outside at -20°C when bad gas are released :p

[Edited on 23-1-2014 by alexleyenda]

Here is my lab

ScienceHideout - 22-2-2014 at 15:10

I promised Pyro a tour, but I kept forgetting... but... I don't break promises, so here it goes!
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200259_zps0cae1c50.jpg" width="800" />
That is the main part of my lab that you see when you walk in.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200358_zpsf375c1fd.jpg" width="800" />
Here is my microscope, it hooks up to the computer. It is one of the Chinese ones, but it works awesome and is of nice quality.

This rolly-cabinet with the rolling door is where I keep my organics. It actually is almost air-tight.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200556_zps093bdf37.jpg" width="800" />
Just a bunch of stuff; including my HUMUNGOUS fire extinguisher.

Above is a counter with a cabinet where I keep my poisons (And burnt out light bulbs).
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200702_zpsccb16e9f.jpg" width="800" />
Fume hood.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200720_zpsfde1c7c1.jpg" width="800" />
Right of the fume hood. Part II on its way.

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[Edited on 22.2.14 by bfesser]

Part II

ScienceHideout - 22-2-2014 at 15:15

<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200730_zps7f782912.jpg" width="800" />
My milligram balance. Ohauses are great, renowned, and reasonably priced.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200741_zps2229eb67.jpg" width="800" />
No... I have never made potassium, and I probably never will.<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200808_zpsd352e193.jpg" width="800" />
Random stuff under my balance table.

I keep a lot of stuff in here including my rock collection and jointware.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_200906_zpsa7065d62.jpg" width="800" />
Example of one of the drawers.
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_201008_zpsa2b09ffd.jpg" width="800" />
Glassware cabinet. Notice Albert Einstein bobblehead. This is not all of my glass. Some of it is dirty and sitting in the sink.

Part III to come

[Edited on 22-2-2014 by ScienceHideout]

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[Edited on 22.2.14 by bfesser]

Part III

ScienceHideout - 22-2-2014 at 15:17

<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_201047_zps37ab129b.jpg" width="800" />
Boring chemicals... Alright, not all of them are boring :D
<img src="http://i1373.photobucket.com/albums/ag387/sciencedean/20140104_201114_zps52e3a16f.jpg" width="800" />
Big bucket holds acids.

That is my lab. Hope you enjoyed :D (That means you, Pyro)

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[Edited on 22.2.14 by bfesser]

zenosx - 23-2-2014 at 20:14

I am jealous of the fume-hood and the storage available! I notice a trend that most of us find that our best chem supplier is elemental scientific. I hope they stay in business for a long time. Based on their backlog, that is hopefully a long way off...

zenosx - 23-2-2014 at 20:14

I am jealous of the fume-hood and the storage available! I notice a trend that most of us find that our best chem supplier is elemental scientific. I hope they stay in business for a long time. Based on their backlog, that is hopefully a long way off...

ScienceHideout - 23-2-2014 at 20:25

Thank you very much! I take pride in both my fume hood and my storage. The way I store my chemicals is state of the art, email me (see my signature) if you want more details.

Elemental Scientific is my favorite. For certain reagents, their prices are unbeatable. HMS beagle and ebay are my second and third favorites :D

Pyro - 24-2-2014 at 04:12

nice lab sciencehideout! I'd love to have a microscope and centrifuge like that!
and that sigma bicarb, don't tell me it's for neutralizing spills! :)

ScienceHideout - 24-2-2014 at 05:19

Lol, funny story about the sigma bicarb... That is actually a jar of peanuts that I ate, cleaned, filled with baking soda, and slammed a sigma label on it :D (Don't tell anyone else, and no one else will know, lol). For some reason labeling is something I am OCD about... The only sigma chemical in my entire lab is the tert-BuOH.

Texium - 8-3-2014 at 13:45

I am jealous of all of these labs… Mine is currently my back yard. Going to get tough in the summer when it gets up to triple digits!

Zephyr - 22-4-2014 at 21:09

The most recent addition to my lab!


aga - 27-4-2014 at 14:16

When is the hole for the water being delivered ?

Zephyr - 27-4-2014 at 16:54

Do you mean the sink? Originally I did not plan on having one, as I have a large lab sink and this would be used mostly for the cooling of condensers. However, when I turn off the water, a substantial amount of water left above the handle pours out. Because of this, I will be installing a small 6" by 4" sink shortly.

mayko - 13-11-2014 at 19:35

Hey I'm back! Had to duck out a while for braincrazies and work, but the good news is...

!!!I HAVE A LAB AGAIN!!!

its_sturdy_I_swear.jpg - 147kB

It began as an abandoned shed. Moving it was hilarious. Myself and several friends unscrewed it from its foundation, moved the foundation, and then got inside and Flinstone-ed it across the yard.

lab1.jpg - 123kB lab2.jpg - 122kB

I'm still unpacking and patching holes and looking around for shelving, etc. But it feels really great to have the space again; it was making me sad to see all my glass and my chems languishing in plastic bins, forming peroxides...

Hope everyone's well; looking forward to being around again!

gardul - 13-11-2014 at 21:20

Not to sound odd here.. but what is with the pentgram?

mayko - 15-11-2014 at 08:42

Quote: Originally posted by gardul  
Not to sound odd here.. but what is with the pentgram?


Pentagrams are awesome and their compass-straightedge construction is fairly easy :D

subsecret - 20-12-2014 at 13:01

Here's my lab, in the basement. The gray cabinet on the right was a server cabinet, and it serves nicely to keep dust off my glassware.

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neptunium - 30-10-2015 at 10:42

Stop working on mine but this is whee it stands now

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arkoma - 16-11-2015 at 06:05

Start of my new setup. Yup, Periodic Table on the wall with a Sharpie, and "Ghetto Balance v3.0"

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[Edited on 11-16-2015 by arkoma]

SteampunkScientist - 16-11-2015 at 11:58

That's a cool balance idea using razor blades! Still, you can get an electronic scale that measures thousandths of a gram on ebay for a few bucks.

I do a lot of electronic experiments, such as high voltage lifters where a balance like that would still be pretty handy...

arkoma - 16-11-2015 at 12:27

I ordered a set of gram masses from eBay today. I wish I could take credit for the razor blade idea, but some rascal thought of it who knows how many years ago. Centuries probably. I'm going to have to put a aluminum blade on one end passing through a gap in a couple of rare earth magnets. Thing takes forever to "zero" because of air currents. Mag field sets up eddy currents which dampen motion. I didna think that one up either *sigh*

*edit*

My balance NEVER needs batteries, nor do I ever wonder, "are the batteries low? can I trust it?"

[Edited on 11-16-2015 by arkoma]

aga - 16-11-2015 at 13:27

... gowever 0.01g balances are probbaly cheaper than the weights, easier to use and the batteries last a very long time indeed.

arkoma - 16-11-2015 at 16:11

to be honest, digital scales remind me too much of selling dope. Been it, no longer in it.

arkoma - 17-11-2015 at 09:57

It's coming along. I managed to get my oil bath to 110C with my re-purposed Bunn-O-Matic coffee warmer

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aga - 17-11-2015 at 10:07

Holy cow !

You're generating elemental Platinum directly onto the periodic table !

[Edited on 17-11-2015 by aga]

j_sum1 - 17-11-2015 at 14:25

You think that is impressive!
It is the great wedge of darmstadium below the platinum that impresses me.

ave369 - 18-11-2015 at 06:23

Quote: Originally posted by gardul  
Not to sound odd here.. but what is with the pentgram?


It's an enchanting station, you noob. For making awesome swords of fire damage.

My own lab is modest compared to what most people have here, especially now during the Russian winter, when it migrated into my living room (because everywhere else is damn cold). It's basically half a table filled with glassware and a wall cabinet with reagent jars. I also had a special acid cabinet, but it failed to migrate into the living room, and right now my acid bottles just stand on the windowsill.

arkoma - 18-11-2015 at 08:18

Quote: Originally posted by ave369  
Quote: Originally posted by gardul  
Not to sound odd here.. but what is with the pentgram?


It's an enchanting station, you noob.


I'm so confused, theologically. My periodic Table is dedicated to Shiva, I mutter to Athena all day long, and I'm going to a local Baptist Church. *sigh*

I don't figure anyone of them has a lock on the "truth"

ave369 - 18-11-2015 at 09:23

Quote: Originally posted by arkoma  

I'm so confused, theologically. My periodic Table is dedicated to Shiva, I mutter to Athena all day long, and I'm going to a local Baptist Church. *sigh*

I don't figure anyone of them has a lock on the "truth"


It has nothing to do with theology. Enchanting stations work on soul gems, and those were made by the Ideal Masters. Who aren't gods, merely frighteningly powerful entities.

Texium - 18-11-2015 at 20:22

Quote: Originally posted by ave369  
Quote: Originally posted by gardul  
Not to sound odd here.. but what is with the pentgram?
It's an enchanting station, you noob. For making awesome swords of fire damage.
Once he figures out that he can use his enchanting station to make Fortify Alchemy apparel which can then be used to craft increasingly powerful Fortify Enchanting potions and so on, we'll all be screwed...

arkoma - 23-11-2015 at 14:29

Got me some good "obtanium" today. Are y'all seeing a fume hood? The squirell cage is an induction motor too, so inherently sparkless.

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The Volatile Chemist - 23-11-2015 at 14:45

Arkoma, Ghetto new balance...
But the Bunnomatic is super-cool, too bad it doesn't get hotter (than meeee...)
I swear, I'll be kicked off the forum someday...
I *just* cleaned up my lab, I'll have to take some pictures now...

arkoma - 23-11-2015 at 15:01

I got my lil' mass set in the mail other day GhettoBalance3.0 works GREAT. Getting ready to knock plumbing through wall from bathroom.

*edit* If I didna have a 16year old daughter, be able to use less "obtanium" (scrounged stuff)

[Edited on 11-23-2015 by arkoma]

[Edited on 11-23-2015 by arkoma]

The Volatile Chemist - 23-11-2015 at 19:01

Heh, Im sixteen. She can handle Vogel and Braums :) Have you taught her chemistry technique yet?
In regards to lab, my lab table is now a piece of family history. Not too smart, but a great table, and mine to keep. The tabletop is a wooden door attached to two handmade short cabinets with drawers. Moveable though, as it dissassembles with ease. Made by my diceased grandfather.
Sorry aboutthe terrible spelling, I'm on a first gen iPod, and it's ten at night...

CharlieA - 23-11-2015 at 19:12

Quote: Originally posted by The Volatile Chemist  


... my lab table is now a piece of family history....The tabletop is a wooden door attached to two handmade short cabinets with drawers... Made by my diceased grandfather.


That's a great story! I have a couple of old tools from my late father-in-law. I treasure them like I'm sure you treasure that lab table.:)

The Volatile Chemist - 28-11-2015 at 08:57

Quote: Originally posted by CharlieA  
Quote: Originally posted by The Volatile Chemist  


... my lab table is now a piece of family history....The tabletop is a wooden door attached to two handmade short cabinets with drawers... Made by my diceased grandfather.


That's a great story! I have a couple of old tools from my late father-in-law. I treasure them like I'm sure you treasure that lab table.:)

Yep. Though I have a piece of glossed wood-board on top of the surface of some of it, and a black plastic-covered piece of cardboard (once the back of a desk calender) covering another part of the surface, so the actual table doesn't get damaged by spills. Funny, both of the chemistry tables I've used have had white surfaces...makes 'em look messy.

Atrum - 29-11-2015 at 00:14

This thread is awesome. So many ideas for my soon to be lab. I only wish I had half of the equipment I have seen in this thread.

ave369 - 30-11-2015 at 03:30

Tadadadadam... Today... The ultra-rare photos of ave369's winter lab! Not the normal lab but the bare bones relocated to the great hall because elsewhere it's too damn cold!




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[Edited on 30-11-2015 by ave369]

[Edited on 30-11-2015 by ave369]

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j_sum1 - 30-11-2015 at 03:35

You inspire me, ave. I thought my lab was cramped and untidy. I don't feel so bad now. :D

ave369 - 30-11-2015 at 03:39

Pay attention to the heating device on the photos. It's the brand new Soviet heating mantle: the Rekord brand pressurized kerosene stove, made back in 1950! And the process of agressive dehydration of the Bat is well underway.

And concerning the chaos in the lab... they don't call me the Mildly Psychoneurotic Scientist for nothing!


Hooray! I've got 85% sulfuric acid! Everything is ready for a Zintl-Karyakin!

Upd: Zintl-Karyakin stopped prematurely because of the uncontrollable bumping. I was afraid that the gunfire-like bumping will break my flask and sprinkle CrO3 all over the place. No boiling chips known to me could stop the bumping.

At least I now have some chromic acid to de-gunk my glassware somewhat. And it was much more de-gunking than doing chemistry. I even used the dreaded nitrochromic acid.

[Edited on 30-11-2015 by ave369]

[Edited on 30-11-2015 by ave369]

ave369 - 30-11-2015 at 05:54

And final hint for everyone: never do the Zintl-Karyakin with ammonium bichromate! The little bitch will decompose in the process of distillation, and all you will get is green sulfuric acid contaminated with chromium trioxide and chromium sulfate!

At least it will work for Glauber's syntheses...

The Volatile Chemist - 2-12-2015 at 12:23

Yum... Nice pics, though a bit too cluttered for me. Good disty-rig, how big is it, actually, it's hard to tell...

arkoma - 17-12-2015 at 06:47


It's coming along. Ain't spending precious cash on ring stands though. My friend made the condenser holder for me out of cypress wood. Inch and a half forstner bit made holes that hold it SNUG. Brought water through the wall from the bathroom. A sink is on the "to do" list.



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Tsjerk - 17-12-2015 at 09:05

Looks nice! How do you hold the two neck flask?

Tsjerk - 17-12-2015 at 09:13

Looks nice! How do you hold the two neck flask?

arkoma - 20-12-2015 at 17:19

Quote: Originally posted by Tsjerk  
Looks nice! How do you hold the two neck flask?


the lovely wood condenser holder keeps it all lined up

UC235 - 20-12-2015 at 17:40

Quote: Originally posted by arkoma  

It's coming along. Ain't spending precious cash on ring stands though. My friend made the condenser holder for me out of cypress wood. Inch and a half forstner bit made holes that hold it SNUG. Brought water through the wall from the bathroom. A sink is on the "to do" list.


I am confused by your blatantly incorrect poster on the wall. Distillation from acidifed dichromate is a standard method of producing aldehydes from alcohols. It would oxidize aldehydes to carboxylic acids with further exposure.

That's a nice martini glass full of vinegar.

j_sum1 - 21-12-2015 at 00:31

Nice setup arkoma. But yes, that poster would annoy me too.

JJay - 21-12-2015 at 03:15

I am going to take a trip to my secret base hidden deep in the salt mines to see if my old lab is still intact. If it is, I should have some photos of some pretty holy equipment to show in a few days. (Or maybe a bunch of broken glass.)

arkoma - 21-12-2015 at 07:07

I know poster is incorrect--it's "tongue-in-cheek". Alcohol is the "solution" to looking at it.

JJay - 22-12-2015 at 03:51

Water got into my electronics... I think I'm going to cry...

Texium - 22-12-2015 at 10:14

I've posted pictures of my lab a few times before, but never in this thread, so I figured it was about time I did.

Lab Bench.JPG - 670kB
First up, my lab bench, with a tiny chloroform distillation in progress.

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Next, the two reagent storage cabinets (organic on the left, inorganic on the right). I also store various odds and ends such as crucibles, stoppers, filter papers, and test papers on the top shelf of the inorganic side.

Centrifuge.JPG - 684kB Drying Rack and Surplus.JPG - 690kB
In one of the cabinets under the bench, I have my centrifuge and a really old variac. My hotplate lives on top of that milk crate when not in use. The other picture shows my glassware drying rack with surplus reagents stored on the shelves underneath.

Glassware-Main.JPG - 455kB Other Glassware.JPG - 508kB
All of my glassware is stored on shelves in my bathroom and bedroom due to lack of space in the garage. Most of it can be seen in these two pictures, but there's a bit more stored away in drawers. A few pop-chem books share a shelf with some in the second picture.

Books and Misc.JPG - 552kB
Here's my collection of chemistry textbooks and references, as well as a bunch of miscellaneous clutter and my compound collection. That's just about everything.

ParadoxChem126 - 22-12-2015 at 10:52

Looks nice, zts. I have the same McMurry fourth edition ochem textbook:D

Zephyr - 22-12-2015 at 11:30

Nice lab zts! I envy those labels and all the cork rings.
I'm renovating my lab at the moment, I think I'll share some photos when it's done.

Texium - 22-12-2015 at 12:05

Thanks guys!
Quote: Originally posted by ParadoxChem126  
I have the same McMurry fourth edition ochem textbook:D
Haha, I found that one at Half Price Books for $4.00

The Volatile Chemist - 30-12-2015 at 14:57

Zts16, nice! How old are you, I always forget; looks very professional. Something to aspire to. Of course you live in a rich-person house, so everything looks pristine (kidding...)


Quote: Originally posted by JJay  
I am going to take a trip to my secret base hidden deep in the salt mines to see if my old lab is still intact. If it is, I should have some photos of some pretty holy equipment to show in a few days. (Or maybe a bunch of broken glass.)

Wait, what... you kidding? If not, that's probably the best thing I've heard all day. That's more to aspire to than a pristine lab, even if the electronics are wet :)

Might as well post pics of the less messy, lab 2.0 for Nathan P. (me...):
That last one's a failed synth of citrazinic acid. Just wanted to throw that crap in here....

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JJay - 30-12-2015 at 16:44

Quote: Originally posted by The Volatile Chemist  
Zts16, nice! How old are you, I always forget; looks very professional. Something to aspire to. Of course you live in a rich-person house, so everything looks pristine (kidding...)


Quote: Originally posted by JJay  
I am going to take a trip to my secret base hidden deep in the salt mines to see if my old lab is still intact. If it is, I should have some photos of some pretty holy equipment to show in a few days. (Or maybe a bunch of broken glass.)

Wait, what... you kidding? If not, that's probably the best thing I've heard all day. That's more to aspire to than a pristine lab, even if the electronics are wet :)

Might as well post pics of the less messy, lab 2.0 for Nathan P. (me...):
That last one's a failed synth of citrazinic acid. Just wanted to throw that crap in here....


Most of the glass was broken too, including my beaker set and most of my boiling flasks. I did recover some ground glass Erlenmeyers.

The Volatile Chemist - 30-12-2015 at 16:46

Quote: Originally posted by JJay  
Quote: Originally posted by The Volatile Chemist  
Zts16, nice! How old are you, I always forget; looks very professional. Something to aspire to. Of course you live in a rich-person house, so everything looks pristine (kidding...)


Quote: Originally posted by JJay  
I am going to take a trip to my secret base hidden deep in the salt mines to see if my old lab is still intact. If it is, I should have some photos of some pretty holy equipment to show in a few days. (Or maybe a bunch of broken glass.)

Wait, what... you kidding? If not, that's probably the best thing I've heard all day. That's more to aspire to than a pristine lab, even if the electronics are wet :)

Might as well post pics of the less messy, lab 2.0 for Nathan P. (me...):
That last one's a failed synth of citrazinic acid. Just wanted to throw that crap in here....


Most of the glass was broken too, including my beaker set and most of my boiling flasks. I did recover some ground glass Erlenmeyers.

...That's crazy...you actually had a lab in some abandoned salt-mines? Wish there were those around here...

JJay - 30-12-2015 at 16:52

Quote: Originally posted by The Volatile Chemist  

...That's crazy...you actually had a lab in some abandoned salt-mines? Wish there were those around here...


No, it wasn't actually in a salt mine...

The Volatile Chemist - 30-12-2015 at 17:00

Quote: Originally posted by JJay  
Quote: Originally posted by The Volatile Chemist  

...That's crazy...you actually had a lab in some abandoned salt-mines? Wish there were those around here...


No, it wasn't actually in a salt mine...

Oh, come now, don't tell such lies... :) Where was it, you have pics?

JJay - 30-12-2015 at 18:21

Quote: Originally posted by The Volatile Chemist  
Quote: Originally posted by JJay  
Quote: Originally posted by The Volatile Chemist  

...That's crazy...you actually had a lab in some abandoned salt-mines? Wish there were those around here...


No, it wasn't actually in a salt mine...

Oh, come now, don't tell such lies... :) Where was it, you have pics?


Hey, when you're a superhero, you don't tell *anyone* where your lab is :D I'll try to post some pictures later, though.

The Volatile Chemist - 30-12-2015 at 18:23

Thanks, looking forward to it.

In case people missed it, pics of my lab 2.0 are the last post on the previous page ;)

Texium - 30-12-2015 at 18:47

Quote: Originally posted by The Volatile Chemist  
Zts16, nice! How old are you, I always forget; looks very professional. Something to aspire to. Of course you live in a rich-person house, so everything looks pristine (kidding...)
Um, thanks, but rich-person house... where'd you get that notion?

The Volatile Chemist - 30-12-2015 at 19:04

Quote: Originally posted by zts16  
Quote: Originally posted by The Volatile Chemist  
Zts16, nice! How old are you, I always forget; looks very professional. Something to aspire to. Of course you live in a rich-person house, so everything looks pristine (kidding...)
Um, thanks, but rich-person house... where'd you get that notion?
Haha, I took a better look and retract my statement.
Sorry if that sounded snob-ish, your lab really does look great.

Texium - 30-12-2015 at 20:01

My family is fairly well-off, but certainly not rich. Most of the glassware that I have was obtained simply by good fortune and chance, as I was able to acquire a ton of nice old glassware from a closed laboratory at no cost. If I showed you the collection of glassware that I've actually spent money on, it would look far less impressive. Consequently, that has allowed me to spend more money on chemicals. The pristine look of everything is just because I am very particular about keeping things clean... especially when I'm getting it prepared to post pictures of it on here. ;)

Work Shop Tour - VIDEO

kadriver - 30-12-2015 at 20:21

Here is a short video of my work shop;

https://youtu.be/0FYgjW-ecRU

Thanks for looking!

kadriver

The Volatile Chemist - 30-12-2015 at 20:22

I see. Sorry about my prior statements. I started my interest in chemistry with the gift of an old chemcraft kit which had lots of rather interesting chemicals and experiments but no glassware except a few test tubes, later I was given old glassware from a man at our church, which included an old style distillation appuratus and 125 mL size things, with more test tubes. More recently, through gift cards given to me, I've purchased chemicals and some general glassware from Home Science Tools. No ground glass yet, I'd love to find some local.
But would you believe it, I can run a vacuum distillation with the glassware I have? :) Buchner flasks are the best, filtration, vac. dist., gas wash bottle.... Good stuff.

Sulaiman - 31-12-2015 at 07:29

here is my shed


4SM_shed.jpg - 2.6MB
table - kitchen door - auxiliary experimentation zone (BBQ & table)- neighbour's house - shed
note the stylish blackout mat ;)

look right


4SM_right.jpg - 2.1MB
chemistry - repairman - electronics - main transceiver (behind wood pile) & telescopes

look ahead


4SM_rear.jpg - 2.3MB
most of my chemicals and glassware
the boxes contain more glassware, bulk dH2O & reagents beneath

hiding from the sun behind the 'chemistry set'


4SM_shy.jpg - 1.8MB

Look Left


4SM_left.jpg - 2.1MB

[Edited on 31-12-2015 by Sulaiman]

Texium - 31-12-2015 at 10:34

Nice shed Sulaiman, looks like you've got a lot of good stuff in there. I see you must do a lot of shopping at Onyxmet. ;)

The Volatile Chemist - 31-12-2015 at 11:23

I was going to say, those looked like onyxmet solvent and reagent liquid bottles :) Very nice. Some fine electronics there!

aga - 31-12-2015 at 11:31

Looks like a busy space Sulaiman.

My main question is how my lucky green underpants got to be on your washing line ?

JJay - 31-12-2015 at 14:44

Here I am running a lab in a public restroom.



20151231_134020.jpg - 792kB

The Volatile Chemist - 31-12-2015 at 15:42

Uh, lol, you kidding? What *are* you making?
Nice lab though :)

JJay - 31-12-2015 at 16:14

Quote: Originally posted by The Volatile Chemist  
Uh, lol, you kidding? What *are* you making?
Nice lab though :)


Ethylsulfuric acid. I am using a technique from a patent that some have stated does not work as claimed... but so far, things have run exactly as expected.


The Volatile Chemist - 31-12-2015 at 16:18

Quite interesting. Did you carry that all in your backpack then set it up in the public restroom? :)

JJay - 31-12-2015 at 18:51

I keep most of my lab equipment and supplies in Sterilite plastic tubs. I have 8 18 gallon tubs and a 40 gallon tub, plus various odds and ends that don't fit in the tubs, e.g. 5 gallon buckets, an ultrasonic humidifier and a small oven.

The Volatile Chemist - 31-12-2015 at 21:36

Cool. It's unfortunate you don't have an actual lab-space. Is that by choice or convinience?

JJay - 31-12-2015 at 22:57

Quote: Originally posted by The Volatile Chemist  
Cool. It's unfortunate you don't have an actual lab-space. Is that by choice or convinience?


Umm, usually I just stick with phone booths and that sort of thing, but they're getting so hard to find these days... anyway, I have to go save a burning village from evil, so later.

JJay - 5-1-2016 at 19:35

I started building a small shed that will serve as a dedicated lab space. Depending on what my work schedule is like this week, I may have it finished tomorrow or perhaps as late as next week.

The Volatile Chemist - 6-1-2016 at 15:57

Nice! Sounds like a good plan. My basement probably isn't the best labspace, but certainly better than nothing.

j_sum1 - 8-1-2016 at 03:09

Ok. My turn.

My lab is a crowded little garden shed in the corner of my place.
DQZVpid.jpg - 1.5MB

The space is shared with gardening stuff, tools, paint, household storage, and, well, everything.
Fy5cbWS.jpg - 1.2MB ilfXcbj.jpg - 1.2MB

The floor is rough-as-guts unreinforced concrete from 60 years ago. Evidently, in a previous incarnation the shed housed some chickens. I bet no one else has fossil footprints in their lab!
sU24MFp.jpg - 1.1MB

After I move the lawnmower out of the way it transmogrifies into the sophisticated lab that it is.
You will notice that I spent the princely sum of zero on shelving for my chemicals. I did get the kids' hand-me-down Ikea tables though. These photos were taken on a day when it was slightly organised. Fire extinguisher and blanket have so far not been needed. But the doorway in close proximity has been useful a couple of times.
Zosde0d.jpg - 1.1MB B4Cjx0Y.jpg - 1.1MB

Glassware is packed neatly into plastic boxes and lives amongst the paint tins.
GcxWkh8.jpg - 1.2MB H0DmI56.jpg - 1.5MB

It's rough, but I do have a decent sized bench to work on.
From left to right on today's mess:
A few beakers awaiting washing
Regulated power supply ready for the next batch of copper sulfate electrolysis
Filtrate from making ferrous oxalate. Coffee filter was too porous so I need to re-do
Jar containing some iodine sediment ready for next time I want to play sublimation with something volatile
Trusty lab book, calculator, scales and the ever-present periodic table
Hotplate with some boiled down sulfuric acid. It is a bit green again from residual copper. I should know by now that I need to give it an extra 10% electrolysis time after it goes clear if I want no coloration.
Glass set up ready for making ammonia solution
Ng3rnhk.jpg - 1.3MB

My lab stands are some concrete reinforcing bar bolted into the desk and rafters.
Scavenged pipette fillers and burettes in the background
IKxbrAR.jpg - 1.1MB

My lab jack is courtesy of a car wrecker's yard. A couple of Nd magnets stuck underneath means that I always know where my stirbars and metal keck clips are.
Rubber bungs are repurposed chair leg protectors from the hardware store.
The can is from SO2 production. The scrappy alfoil pans are from New Year's coloured flames. I don't really want to throw out my strontium salts but it will take some work to get them clean again.
bCEc0bL.jpg - 1.3MB


In the future I intend to construct a fume hood. You know all those experiments that should be done "outside or in a fume cupboard"? Ironically, my fume cupboard will be outside. It won't be the better for it but it really is the only option. I guess I am building a little shed-let to sit beside the main shed.

DQZVpid.jpg - 1.5MB

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