Quote: Originally posted by PHILOU Zrealone | Quote: Originally posted by XeonTheMGPony | Interesting story as I had to make more HMTD for my caps, here for some reason drying any thing is a tedious proposition at best and was tempted to
vacuum filter it on my fritted funnel.
But When I did the risk analysis first thing on the list was just that! getting it off the frit was just way to high risk a venture, and too much
containment in the funnel made it more like a grenade then a filter method. So scratched the idea and here it is 3 days later still drying on the open
coffe filter!
Going to be making a temperature gradiated vacuum desiccator for these things to make it berable |
Worst case scenario must always be kept in mind...
Glass shrapnells cut and pierce flesh...hard plastic too...just like metal or wood...in close viccinity
So better think to safer soft plastic beakers...in the case of a bad event...consequences will be less.
With peroxydes, the worst is always to be feared so tiny quantities is a must...
Special care to this since with the cheap price of inital ingredients, one often puts 50-100ml easily into reaction and gets finally 50-200g of final
product...what is totally irresponsible (I speak from experience with CTAP although I had no bad event, I was uncomfortable with the amount of
crystals it produced)...
[Edited on 16-11-2016 by PHILOU Zrealone] |
Growing up in a remote logging camp you learn fast that if you do not think you die (Same for panic, you panic you die, every one should say this to
them selfs morning and night, you can panic after wards but befor it will be the end of you), I find my self even running risk analysis when just
making coffee, it truly is a mind set of thinking.
If I do this, how can it go wrong, and when it does what injuries could I receive, can it cause fire or vapor, so on.
It has saved me allot of times int he energetic's end of it, you get impatient and want to rush some thing then that little subroutine slams the
breaks on and waves that Darwin award in front of you screaming "NOMINATED!"
Then you step back and realize had ya don it you'd be cleaned up with a sponge or what have you. As a kid saved a few people back in school too who
would be missing some hands. All ways check your fuses for dusting of primary powder! Can't do its job when the flame has a short cut!
As for plastic at those forces glass / plastic is the same, the only safe thing is very care full and diligent procedure and distance and never work
when you're tired or low blood sugar.
All my EM work is don in the noon after my after lunch nap! Fully awake alert and fed, that alone lowers risk hugely. |