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Distillation Setup for 1,4-Butanediol to gamma-Butyrolactone
Len, I don't see what is your concern. Over the years I have spoken with others in u2u, email etc. o ...
8-1-2010 at 05:22
by: sonogashira
Drying alcohols with Sodium Glycoxide
Thanks very much!
7-1-2010 at 15:52
by: sonogashira
Acid Base Chemistry (H2SO4 + Na2OOCCH3)
^Maybe it could help to add salt to the water-bicarbonate wash do you think? It may help to dry the ...
7-1-2010 at 03:21
by: sonogashira
caffeine hcl salt
[rquote=168679&tid=13194&author=Satan]In health preparations in my country, to increase its ...
7-1-2010 at 02:29
by: sonogashira
Drying alcohols with Sodium Glycoxide
[rquote=169038&tid=13212&author=Nicodem]It is even simpler to prepare sodium isopropoxide.[/ ...
7-1-2010 at 02:17
by: sonogashira
Polyaniline
Dimethyl sulfone (DMSO2), sold in health stores, is a very good polar aprotic solvent. Unfortunately ...
4-1-2010 at 05:59
by: sonogashira
The short questions thread (2)
Oh I see :) Maybe I implied that - but really I meant the exact opposite! I thought perhaps you knew ...
2-1-2010 at 10:10
by: sonogashira
caffeine hcl salt
[rquote=168661&tid=13194&author=ronnymac]I bought several grams of caffeine but it is not ve ...
2-1-2010 at 03:06
by: sonogashira
The short questions thread (2)
Thank you Panache - unfortunately in this case the freezing point of acetophenone is 20 C (although ...
2-1-2010 at 02:45
by: sonogashira
Fine old instruments
Thank you! I forgot about the lighting issue. I think I won't tell him to get an antique then... but ...
1-1-2010 at 03:23
by: sonogashira
The short questions thread (2)
Hey, thanks very much! You're right, there will be a small amount of acetone co-solvent (few ml), bu ...
1-1-2010 at 03:03
by: sonogashira
The short questions thread (2)
Thanks. It is the (expected) product ratio from the oxidation of styrene with H2O2 and palladium chl ...
31-12-2009 at 11:22
by: sonogashira
The short questions thread (2)
[rquote=166911&tid=12054&author=Nicodem][rquote=166544&tid=12054&author=sonogashira] ...
31-12-2009 at 09:53
by: sonogashira
Fine old instruments
It is very nice :)

Can I ask you though - do you think it is as good as a more modern microscope ...
31-12-2009 at 09:39
by: sonogashira
Concentrations of a few "Household" Chemicals
Don't think I have ever seen a robert dyas shop :( Maybe I will look in a larger wilkinson store bec ...
29-12-2009 at 16:18
by: sonogashira
Concentrations of a few "Household" Chemicals
^ It was the sulphuric acid I was asking about :P A lot of caustic soda your right, but suplhuric ac ...
29-12-2009 at 10:52
by: sonogashira
Concentrations of a few "Household" Chemicals
[rquote=167980&tid=1247&author=Picric-A]The Drain unblocker we buy in the UK ( i buy from Wi ...
29-12-2009 at 10:07
by: sonogashira
Laboratory Tips and Tricks
^ Yes, I think that is used as a nicer form of Br2 (the ethene goes)
27-12-2009 at 06:43
by: sonogashira
Laboratory Tips and Tricks
Not-quite in answer to a question above... But still, a 'tip' :)

[u]Br2 is better than I2 for sta ...
27-12-2009 at 05:25
by: sonogashira
Acid Base Chemistry (H2SO4 + Na2OOCCH3)
This is from page 66 of Norris - Experimental Organic Chemistry (from forum library I think...)
Mos ...
26-12-2009 at 03:01
by: sonogashira
Indole Synthesis
[rquote=168115&tid=13152&author=Satan]From 5-methoxyindole, melatonin can be made, it would ...
26-12-2009 at 02:47
by: sonogashira
Diethyl Ether - Illustrated Practical Guide
Wow! I am jealous of all this equipment!

But I wondered: does 'wet' ether form a peroxide also? W ...
25-12-2009 at 18:40
by: sonogashira
Indole Synthesis
It is acid-catalysed reaction, so anything resistant to decoposition by acid (amines, carboxylic aci ...
22-12-2009 at 12:37
by: sonogashira
Benzyl chloride from Benzyl acetate
Maybe acetate can be used as a leaving group to save need for conversion to chloride?
22-12-2009 at 08:12
by: sonogashira
Australian Internet Filtering Passed (The Books Are Burning)
Oh, forgive me, I thought it was from the start... Though I only read one book and that was maybe 8 ...
20-12-2009 at 16:09
by: sonogashira
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