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Hydroxylamine Production
I would be dead by the amount of inhaled. I was at work. (i work at this shithole im only 15) It was ...
30-1-2005 at 15:06
by: PainKilla
Diphoronepentaperoxide (DPPP)
Actuallly that is intersting, I would like to see what happens with ketones in general because perha ...
30-1-2005 at 14:55
by: PainKilla
Acetone Experiments
Ah, thank you very much, those are very intersting especially the first one. I need to get some lime ...
30-1-2005 at 14:51
by: PainKilla
Diphoronepentaperoxide (DPPP)
Well, I got no small amount of crystals etiehr, I have maybe 2mm of liquid and the rest is a slur of ...
30-1-2005 at 14:15
by: PainKilla
Hydroxylamine Production
I am wodnering how to make this useful compound... here is a few ideas:

NaOCl + NH4OH --> NH2C ...
30-1-2005 at 14:04
by: PainKilla
Diphoronepentaperoxide (DPPP)
I am trying to see what effect other chemicals ahve on acetone, like H2SO4 vs HCl. I am trying to se ...
30-1-2005 at 13:59
by: PainKilla
Diphoronepentaperoxide (DPPP)
Yes, I agree, but I do think we should at least make some sort of new thread or maybe a document wit ...
30-1-2005 at 13:42
by: PainKilla
Acetone Experiments
Intersting, do you have any direct references to this? I say it only because it is of much interest ...
30-1-2005 at 13:35
by: PainKilla
Diphoronepentaperoxide (DPPP)
I am gonna filter out my "DPPP" soon. I think giving it a new name would be approtiate als ...
30-1-2005 at 13:33
by: PainKilla
Acetone Experiments
In conjuction with the DPPP thread here is some interesting resutls I have attained:

Acetone + HC ...
30-1-2005 at 10:52
by: PainKilla
Diphoronepentaperoxide (DPPP)
Lol, that is what I said too, but nooone lsitens. I am going to filter out my stuff later today hope ...
30-1-2005 at 09:50
by: PainKilla
Diphoronepentaperoxide (DPPP)
I did everything the same as the HCl method jsut replaced the acids.... It wil be filtered soon but ...
29-1-2005 at 17:37
by: PainKilla
Diphoronepentaperoxide (DPPP)
If I made something using H2SO4 then no Cl is nessacary, therefore disproven....

[Edited on 30-1-20 ...
29-1-2005 at 17:15
by: PainKilla
Diphoronepentaperoxide (DPPP)
I thought the theory with chlorination has been disproved already? Will someone neutralize thier mix ...
29-1-2005 at 16:44
by: PainKilla
Diphoronepentaperoxide (DPPP)
I used NaHCO3 to neutralize. Regarding your probelm understanding the pwoer....


Brisance is bas ...
28-1-2005 at 16:31
by: PainKilla
Diphoronepentaperoxide (DPPP)
I am quite puzzled right now, I neutralized one of my mesitylene oxide, and it lost all of its color ...
28-1-2005 at 16:11
by: PainKilla
Diphoronepentaperoxide (DPPP)
I don't think that it matters what color it is. It's just the darkening of the mesityl oxi ...
28-1-2005 at 15:54
by: PainKilla
IMPORTANT ANNOUNCEMENT
This is room temperature, in a sealed flask. I will wait 7 days and see what happens. Depending how ...
28-1-2005 at 10:05
by: PainKilla
urea perchlorate
I remember trying to find a way to do it myself but coudln't find one. Ill try to pull up a few ...
28-1-2005 at 09:49
by: PainKilla
urea perchlorate
It probably doesn't exist, on top of that it is damn near impossible to get HClO4 from KClO4. Y ...
28-1-2005 at 09:29
by: PainKilla
Diphoronepentaperoxide (DPPP)
[quote][i]Originally posted by Matsumoto_Hideki[/i]
Painkilla during all of our synth methods the y ...
28-1-2005 at 09:17
by: PainKilla
Diphoronepentaperoxide (DPPP)
OK, I hate snow. I am in the process of doing the first part of my experiment. 30% H2SO4 (to equal 3 ...
27-1-2005 at 16:37
by: PainKilla
Diphoronepentaperoxide (DPPP)
Ah I see you used the SnCl2 way, but you msut take into account that not only TeAP was formed. I thi ...
25-1-2005 at 20:53
by: PainKilla
Diphoronepentaperoxide (DPPP)
The only REAL TeAP i have seen is with the use of SnCl4 for even decent yeilds. I ahev not seen any ...
25-1-2005 at 20:30
by: PainKilla
Diphoronepentaperoxide (DPPP)
The purpose of this experiment is to possibly eliminate the phorone part (i dont beleive its possibl ...
25-1-2005 at 20:07
by: PainKilla
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