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Possible easy thionyl chloride synthesis
Yeah, phosgene is no joke. There was an extra special safety training required by my university when ... |
11-12-2019 at 05:34
by: Metacelsus |
Allyl Bromide Preparation
[rquote=627769&tid=154557&author=Pumukli]
Why is substitution of the OH with Br is preferre ... |
11-12-2019 at 05:26
by: Metacelsus |
Diethylamine and m-Toluic acid from DEET
[rquote=627588&tid=154530&author=Boffis]@Metacelsus, That's a good point and I'll fix it whe ... |
8-12-2019 at 05:41
by: Metacelsus |
Diethylamine and m-Toluic acid from DEET
Very cool! Just a minor nitpick: you often write "M" which means "molar", where you mean moles. For ... |
7-12-2019 at 14:37
by: Metacelsus |
Invitation to Participate in a Research Study
Sounds interesting. I will participate. |
4-12-2019 at 05:17
by: Metacelsus |
What would the procedure for Benzidine to aniline look like?
In particular, the benzidine is metabolically acetylated and oxidized to an N-hydroxy compound, whic ... |
27-11-2019 at 05:18
by: Metacelsus |
Christmas is approaching , any ideas ?
[rquote=626406&tid=154448&author=j_sum1]Red and green flames using copper / boric acid / bar ... |
26-11-2019 at 12:31
by: Metacelsus |
1-chloro-2-propanone (chloroacetone)
1) What's the beautiful red compound formed when chloroacetone is added to NaOH?
From experience: ... |
25-11-2019 at 17:11
by: Metacelsus |
Methoxy-EthylTryptamine
Wolff-Kishner reductions are for ketones and aldehydes, not amides. Your plan is doomed to fail.
... |
21-11-2019 at 04:50
by: Metacelsus |
Energetic precipitate from the reaction of ascorbic acid/Cu(II) and sodium nitrite
[rquote=626130&tid=154430&author=nitro-genes]Since all of the copper was removed from the re ... |
17-11-2019 at 05:17
by: Metacelsus |
Thionyl chloride from batteries
A laptop battery almost certainly won't have SOCl2 (or even any metallic lithium). Only non-recharge ... |
13-11-2019 at 04:31
by: Metacelsus |
Tried to synthesise Disodium hydrogen phosphate from red phosphorus and sodium hydroxide
Yes it should produce the salt (the initial product would be P2O5 which would then dissolve).
But ... |
12-11-2019 at 20:08
by: Metacelsus |
Troubleshooting Zn/HCl reduction of nitrostyrenes
Some years ago I tried that same procedure exactly as written. It didn't work (although the starting ... |
12-11-2019 at 20:03
by: Metacelsus |
Thiosulfate Dietary Supplement?
[rquote=625836&tid=154318&author=hodges]
Supposedly oxidation contributes to health issues ... |
11-11-2019 at 05:00
by: Metacelsus |
Questions about extraction methods
None of them except maceration (and Soxhlet extraction, if you have the apparatus) are simple.
Th ... |
10-11-2019 at 05:52
by: Metacelsus |
Glycated hemoglobin, HbA1c levels
Hmmm, maybe some water was lost by the time of the third measurement, and the concentration was ther ... |
6-11-2019 at 17:33
by: Metacelsus |
Oxidising uric acid?
Not a nitrosamine but a nitroamine (N-NO2). Nitrosamines have formula N-NO
I don't know of any go ... |
31-10-2019 at 18:46
by: Metacelsus |
Glycated hemoglobin, HbA1c levels
The reaction is Schiff base formation followed by https://en.wikipedia.org/wiki/Amadori_rearrangemen ... |
30-10-2019 at 03:27
by: Metacelsus |
Readily Available Chemicals Website: Version 2
I archived it here: https://archive.md/OdSl
edit: not sure if that also archived the subpages
[E ... |
29-10-2019 at 19:14
by: Metacelsus |
Why some compounds may disappear in TLC?
Sometimes compounds react with silica gel and decompose. |
29-10-2019 at 04:37
by: Metacelsus |
Synthesis of a Highly Fluorescent Boron subporphyrazine
Very cool! And I'm glad your GF likes science 
Is the blue solution fluorescent? |
26-10-2019 at 04:05
by: Metacelsus |
high sensitivity low explosives
[rquote=624897&tid=154209&author=Pyro_cat]Off topic but its on my pyro bucket list, never go ... |
24-10-2019 at 06:48
by: Metacelsus |
The Short Questions Thread (4)
[rquote=624886&tid=25055&author=artemov][b]Question[/b]
Is 70%-80% sulfuric acid any usef ... |
24-10-2019 at 06:46
by: Metacelsus |
PTFE filters? What are they for?
[rquote=624739&tid=153515&author=RogueRose]
[b]" D - Severe"[/b]
Diethylamine
Fluorine
... |
21-10-2019 at 15:13
by: Metacelsus |
Extraction microrna From Humans Plasma
Trizol should work, but under some conditions low GC miRNAs could be lost. Make sure to use appropri ... |
21-10-2019 at 04:02
by: Metacelsus |
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