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Ethane Sulfonyl Chloride Synthesis
If you have access to dimethyl sulfoxide then chlorination affords methanesulfonyl chloride ([i]aka[ ... |
7-3-2016 at 08:12
by: DJF90 |
fluid pump and tubing capable of pumping low temperature 0C to -78C temp Acetone
[rquote=441014&tid=65523&author=quantumcorespacealchemyst]
i am unsure how to go about it. ... |
7-3-2016 at 07:55
by: DJF90 |
What's the best way to recover Pd from Pd-Organic complexes?
[rquote=440554&tid=65474&author=Dr.Bob]This is a good question, I have collected much Pd cru ... |
2-3-2016 at 16:13
by: DJF90 |
Fractional distillation questions
@Magpie - The OP specified the scale of distillation:
[rquote=440594&tid=65481&author=jem ... |
2-3-2016 at 13:36
by: DJF90 |
Ibuprofen - Methyl ester and hydroxamic acid derivatives
@Av - If you have more work planned with Ibuprofen then perhaps (if Nicodem and yourself agree) it c ... |
1-3-2016 at 04:57
by: DJF90 |
Ibuprofen - Methyl ester and hydroxamic acid derivatives
I'd like to congratulate you on an exceptionally clear and well written report. I like how you confi ... |
29-2-2016 at 04:52
by: DJF90 |
n-amyl alcohol
[rquote=440092&tid=65422&author=UC235]I find it rather interesting that every intro organic ... |
27-2-2016 at 17:32
by: DJF90 |
Schmidt reaction - advice on solvents
I hope you're not asking for answers to a commercial or academic problem on an amateur science forum ... |
26-2-2016 at 02:35
by: DJF90 |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
[rquote=439909&tid=65075&author=Nicodem]
It's just that I'm flooded with work and could no ... |
25-2-2016 at 12:25
by: DJF90 |
Detection of Toxic Gasses
Nitrogen dioxide is also detected by starch iodide paper according to the equation:
2KI + 2NO2 =& ... |
25-2-2016 at 11:58
by: DJF90 |
3-nitrophthalic acid fail (EVERY TIME)
Are you using a reflux condenser? Nitric acid boils at 83 *C |
25-2-2016 at 03:37
by: DJF90 |
Detection of Toxic Gasses
[rquote=439823&tid=65397&author=SmellNoEvil]
I would like a reliable way to detect them whe ... |
24-2-2016 at 15:32
by: DJF90 |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
[rquote=439725&tid=65075&author=Nicodem]A lot of talk instead of doing an experiment. Like t ... |
24-2-2016 at 11:17
by: DJF90 |
Solubility Data
On closer inspection some of the articles are behind a paywall... But thanks for bringing it to our ... |
24-2-2016 at 07:59
by: DJF90 |
Someone experience with Cycloalkenes to cyclocarbonyls
[rquote=439675&tid=65376&author=UC235]
Actually, this can be done in the liquid phase (perh ... |
23-2-2016 at 01:58
by: DJF90 |
Grignard successes and failures
[rquote=439490&tid=65348&author=fluorescence]
So if anyone plans to do his grignard using ... |
21-2-2016 at 09:03
by: DJF90 |
1,4-Dioxane from Ethylene Glycol and H2SO4
[rquote=439269&tid=65311&author=DJF90]
Cheers for the reference Av, I've requested it at th ... |
19-2-2016 at 13:04
by: DJF90 |
1,4-Dioxane from Ethylene Glycol and H2SO4
[rquote=439256&tid=65311&author=AvBaeyer]If you can get access to Elderfield's "Heterocyclic ... |
19-2-2016 at 03:36
by: DJF90 |
1,4-Dioxane from Ethylene Glycol and H2SO4
[rquote=439210&tid=65311&author=UC235]I've done this before. Workup is complicated by:
1) ... |
18-2-2016 at 14:52
by: DJF90 |
amide and nitrous acid?
[rquote=438946&tid=65321&author=Cheddite Cheese]Short answer: no, it won't.
Long answer: ... |
15-2-2016 at 04:14
by: DJF90 |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
[rquote=438853&tid=65075&author=AvBaeyer]
I watched your video and it was an interesting ex ... |
14-2-2016 at 02:32
by: DJF90 |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
For the benefit of the OP here is a link to the mentioned Iodomethane thread in Prepublications:
... |
9-2-2016 at 09:40
by: DJF90 |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
[rquote=438195&tid=65075&author=blogfast25]
Primary alcohols can't be halogenated with HX [ ... |
9-2-2016 at 04:45
by: DJF90 |
anhydrous formaldehyde
I posted a paper elsewhere on the forum not too long ago regarding the preparation of monomeric form ... |
9-2-2016 at 01:14
by: DJF90 |
Collidine vs Pyridine
[rquote=436748&tid=65126&author=numos]
It wouldn't even be a problem, I could just test it, ... |
25-1-2016 at 22:06
by: DJF90 |
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