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Complete Rhodium archive found on eMule !
The above Rhodium archive contains 264 pdfs totalling 190 MB if I counted correctly.
Since I have t ...
4-8-2005 at 17:34
by: S.C. Wack
What do to with KMnO4?
Reactions of KMnO4 with propylene glycol, ethylene glycol, acetaldehyde, ethanol, acetone, IPA, glyo ...
3-8-2005 at 16:35
by: S.C. Wack
Palladium on Charcoal 5%.
Go here:
http://pubs3.acs.org/acs/journals/toc.page?incoden=jacsat&indecade=4&involume=84&a ...
2-8-2005 at 20:22
by: S.C. Wack
Things to do with Nickel
The above reductions by Raney alloy collection of articles was uploaded too soon, I have [url=http:/ ...
2-8-2005 at 19:14
by: S.C. Wack
Raney alloy
THE SKIP THIS, ITS OFF-TOPIC PART:
I was having a little discussion with ning at WD some months ago ...
31-7-2005 at 11:36
by: S.C. Wack
toluene --> benzaldehyde
solo: My question was, why would the benzaldehyde formed not react with the conc. hydroxide the seco ...
27-7-2005 at 17:14
by: S.C. Wack
toluene --> benzaldehyde
Yield? Why no Cannizzaro?
27-7-2005 at 14:11
by: S.C. Wack
FREE Online Journals
Guess it should be mentioned here that the first page of all pre-1996 ACS articles are free - in cas ...
27-7-2005 at 13:02
by: S.C. Wack
Benzoic Acid, Carbamid>Benzamid>Anilin?
Not urea, but since I'm posting aniline experimentals here and this is not interesting enough t ...
26-7-2005 at 17:39
by: S.C. Wack
Benzoic Acid, Carbamid>Benzamid>Anilin?
Excerpt from Helv. Chim. Acta 29, (1946) pp. 1440-1:

Exemples d'acidolyse de l'urée.
...
25-7-2005 at 17:39
by: S.C. Wack
Solubility of chromium sesquioxide (Cr2O3)
It is alleged in several books that it can be mostly dissolved by fusion with persulfate or pyrosulf ...
25-7-2005 at 17:35
by: S.C. Wack
15% peroxyacetic stoichiometry question.
I know nothing of the best way to make the most concentrated peracetic acid from 27% H2O2 and haven& ...
24-7-2005 at 22:27
by: S.C. Wack
3,4,5-trimethoxy-beta-nitrostyrene synthesis
Yes, phenylacetaldehyde is more interesting for some, not benzaldehyde itself. I too have read the O ...
24-7-2005 at 21:51
by: S.C. Wack
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
On a slightly less than 1 gram scale:
24-7-2005 at 19:51
by: S.C. Wack
3,4,5-trimethoxy-beta-nitrostyrene synthesis
I'm not even sure that it would work on pyrogallol, I have no refs.

This is something that I ...
24-7-2005 at 10:44
by: S.C. Wack
New chemistry forum for Hive Bees
[url=http://www.google.com/search?num=30&hl=en&lr=&as_qdr=all&q=synth78+site%3Awww.w ...
23-7-2005 at 11:26
by: S.C. Wack
Link database?
It is not that hard. Well, it depends on what you want and how you're set up.
Advertising a ch ...
22-7-2005 at 20:13
by: S.C. Wack
Organic Hypochlorites
And once you do have the hypochlorite, what can you do with it, other than chlorinating amines as in ...
21-7-2005 at 14:09
by: S.C. Wack
3,4,5-trimethoxy-beta-nitrostyrene synthesis
Methyl iodide is specifically mentioned in Vogel. Methyl bromide can methylate pyrogallol and syring ...
20-7-2005 at 10:58
by: S.C. Wack
Phosphoric acid etching??
Not sure that I understand the question. Hot concentrated H3PO4 dissolves SiO2, not fast.
20-7-2005 at 10:08
by: S.C. Wack
IPA and peroxides
Alter ego post:

https://www.synthetikal.com/synthforum/about1265.html
19-7-2005 at 20:55
by: S.C. Wack
Ethyl ether distillation and synthesis
Here is a JACS article where Et2O or ethylene (depending on whether the temp is 250 or 350) is made ...
17-7-2005 at 20:13
by: S.C. Wack
Tear gas from SO2Cl2 + LiOMe?
In this 1919 French article, the authors did not get much methyl sulfate by heating Na or K methyl s ...
14-7-2005 at 21:10
by: S.C. Wack
toluene --> benzaldehyde
Just a little addition to the Mn acetate/toluene electro-abstracts. Can't believe I missed this ...
11-7-2005 at 18:06
by: S.C. Wack
PbO2
Yes, that process has been known for a very long time - as a preparation of basic lead carbonate &qu ...
10-7-2005 at 22:02
by: S.C. Wack
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