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home brew silica supported hydrogenation catalysts
DJF90- I dont have any catalyst left from the first batch but I do still have all the precursors nec ... |
22-3-2011 at 13:43
by: mnick12 |
Nitroethane from ethylsulfate, Desseigne variation.
Im sorry I dont remember the yields from the reaction of NaHSO4 with ethanol, but if I remember corr ... |
22-3-2011 at 13:13
by: mnick12 |
home brew silica supported hydrogenation catalysts
Hello everyone heres what I have been working on lately, its a continuing project and I am open to s ... |
21-3-2011 at 20:11
by: mnick12 |
Nitroethane from ethylsulfate, Desseigne variation.
Im not sure if anyone is interested but I will post anyway.
There is some patent floating around ... |
21-3-2011 at 19:55
by: mnick12 |
Separating TCCA and Calcium Hypochlorite
I doubt its 48% Ca(ClO)2 and 52% TCCA, that mixture of chemicals would be highly unstable. Im pretty ... |
9-3-2011 at 17:57
by: mnick12 |
eugenol -->vanillin
Huh?
The reason why one isomerizes eugenol to isoeugenol is so that the double bond can be cleaved ... |
28-2-2011 at 21:06
by: mnick12 |
Making fire (youtube collaborative video)
I remember trying a variant of this a couple of years ago. I didnt have any brake fluid so I thought ... |
23-2-2011 at 20:41
by: mnick12 |
NiO as hydrogenation catalyst?
Sedit, it is interesting that you bring up that patent. A couple of weeks ago I was investigating a ... |
23-2-2011 at 20:34
by: mnick12 |
Protecting phenols in a grignard reaction
Sounds like benzyl ether is the way to go!
@Chordate: I can get 5% Pd on C, 10% Pd on Alumunia, 5 ... |
23-2-2011 at 16:36
by: mnick12 |
Protecting phenols in a grignard reaction
So some time in the near future I would like to prepare a Grignard from m-bromophenol, but that OH i ... |
22-2-2011 at 17:22
by: mnick12 |
Preparation of 1-bromo-3-nitrobenzene
A little update.
I ran the synthesis of nitrobenzene found on Vogel, but instead of a steam bath I ... |
21-2-2011 at 20:35
by: mnick12 |
toluene --> benzaldehyde
HV does indeed produce ozone, have you ever messed around with a moniter flyback transformer?
Tw ... |
15-2-2011 at 19:42
by: mnick12 |
Preparation of 1-bromo-3-nitrobenzene
Thank you for both of those papers, they are very interesting. I am however particularly interested ... |
15-2-2011 at 19:31
by: mnick12 |
Preparation of 1-bromo-3-nitrobenzene
So here is a problem that I need help with. Lately I have been looking for ways to synthesize small ... |
14-2-2011 at 20:21
by: mnick12 |
Oxidation of Ethanol to Ethanal?
Oh boy, if you are not sure what mechanism means then I am afraid any attempt to explain the oxidati ... |
7-2-2011 at 20:29
by: mnick12 |
Oxidation of Ethanol to Ethanal?
what is what? |
7-2-2011 at 20:17
by: mnick12 |
Oxidation of Ethanol to Ethanal?
This took me a gut-wrenching 3 minutes to find: http://www.springerlink.com/content/u14n74051g547p07 ... |
7-2-2011 at 20:09
by: mnick12 |
Cap design
Well shrapnel tends to fly in ever direction now matter how the explosive detonates. In an ideal wor ... |
7-2-2011 at 20:01
by: mnick12 |
cover for cathode back suggestions ?
I have had some luck protecting my iron cathodes using 200-500mg of chromic acid or some dichromate ... |
16-1-2011 at 12:34
by: mnick12 |
Is this KNO3 source reliable ?
They look pretty good, but can you find KNO3 locally? In the US it is available as stump remover in ... |
4-1-2011 at 12:50
by: mnick12 |
Alkoxide salts
I prepared some lithium methoxide a while ago from lithium foil (the stuff from batteries) and prett ... |
3-1-2011 at 17:35
by: mnick12 |
N-methyl isopropylamine synthesis
While I have not had any expirience with N-methylisopropylamine most amines tend to have a fishy "de ... |
27-12-2010 at 22:18
by: mnick12 |
ethane sulfonyl chloride STENCH
Sounds like your bunte salt hydrolized into ethanthiol, I think the best way to get rid of that smel ... |
26-12-2010 at 14:05
by: mnick12 |
can a computer power supply kill you?
Current varies inversely with resistance, so as the resistance goes down then the current goes up. O ... |
25-12-2010 at 01:40
by: mnick12 |
catching H2S
I have seen alot of people use lead nitrate to absorb hydrogen sulfide, but then you have to deal wi ... |
22-12-2010 at 22:09
by: mnick12 |
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