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Hydrobenzofuran ring formation by cyclisation of 2-phenoxy-ethanol Interesting idea. I could only find the reference what you already found. To say the least I doubt i ... |
25-5-2020 at 09:26 by: Pumukli |
2,4-dihydroxybenzoic acid from resorcinol Fery,
I think even a decomposition test would be meaningful (=confirmation of the identity and mayb ... |
25-5-2020 at 06:20 by: Pumukli |
So called Maple Lactone Good find, Boffis!
Try the ring contraction at first. It would be interesting in itself if worked ... |
25-5-2020 at 02:54 by: Pumukli |
2,4-dihydroxybenzoic acid from resorcinol Nice synths, Fery!
A melting point determination would be nice too. Doesn't matter, if it decompo ... |
25-5-2020 at 02:15 by: Pumukli |
Salicylic acid methylation? Thanks dawt!
So it seems it can be done.
Maybe the ester would be OK too.
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24-5-2020 at 22:58 by: Pumukli |
Salicylic acid methylation? I've been wondering how easy was the methylation reaction of salicylic acid?
No, not the esterifi ... |
24-5-2020 at 04:32 by: Pumukli |
Anthranilic acid preparation(questions) Depending on your aim, preparing isatoic anhydride might actually be a more desirable goal.
Edit ... |
7-5-2020 at 23:58 by: Pumukli |
Cubane instead of benzene with the phenylethylamine backbone Cyclopentanone is somehow more aggressive towards living tissue than say cyclohexanone! Severe eye i ... |
19-1-2020 at 11:11 by: Pumukli |
OTC Dimethyl Ether "found a pretty chill Methylating agent for future reference"
Really? What can be methylated by D ... |
6-1-2020 at 11:31 by: Pumukli |
Announcements of Articles in Progress Unfortunately after my announcement life intervened and I'm in quite a turmoil in these days. I regr ... |
2-1-2020 at 10:18 by: Pumukli |
Tech grade NaBr smells Are you sure you smelled H[sub]2[/sub]S?
What if the cause of the smell is Br[sub]2[/sub] in low ... |
30-12-2019 at 07:43 by: Pumukli |
Organic Electrochemistry Questions These E(1/2) values (or E.m.f-s) are referenced to the so called standard hydrogen electrode (Google ... |
24-12-2019 at 14:19 by: Pumukli |
Hydrochloric acid separation Maybe you should try the suggested two pot method! It does not require distillation only time.
It ... |
22-12-2019 at 22:13 by: Pumukli |
Help in synthesising manganese (II) sulfate You can safely forget the peroxide route.
In my experience MnO[sub]2[/sub] is such an efficient cat ... |
18-12-2019 at 22:37 by: Pumukli |
FC alkylation? If your goal is ethylbenzene then forget FC alkylation. It produces a mixture (due to "overalkylatio ... |
17-12-2019 at 10:03 by: Pumukli |
Crap from "attempt to make isopropyl salicylate, something interesting happened" A few drops of sulfuric acid should be enough, with much longer reflux time (8-10 hours). (It works ... |
16-12-2019 at 06:01 by: Pumukli |
Using conc H2SO4 + NaCl to chlorinate alcohols? It will work, (Lucas' reagent.)
What won't work (probably) is your original idea (mixing sulfuric ... |
16-12-2019 at 05:43 by: Pumukli |
if you need ethanol, do you get denatured ethanol, or 190 proof everclear? Thanks! I tried something like that, a method to detect acetone (and MEK) in urine, is reportedly se ... |
15-12-2019 at 23:24 by: Pumukli |
Haloform Reaction With Ca(OCl)2 and EtOH Expect some chlorine on acidification! |
15-12-2019 at 23:21 by: Pumukli |
Using conc H2SO4 + NaCl to chlorinate alcohols? Can we make i-propyl-chloride from HCl and i-propanol?
(Because your suggested method is basicall ... |
15-12-2019 at 23:18 by: Pumukli |
Report on making Copper iodide Great!
The colour looks good, yes.
I thought these Cu+ compounds are more sensitive to oxidation i ... |
15-12-2019 at 07:49 by: Pumukli |
if you need ethanol, do you get denatured ethanol, or 190 proof everclear? You seem to be more successful with this purification than me. Although the fine print on the label ... |
15-12-2019 at 07:35 by: Pumukli |
Haloform Reaction With Ca(OCl)2 and EtOH There's a warning somewhere in this forum in circulation that reminds people of the possible explosi ... |
15-12-2019 at 07:18 by: Pumukli |
Yellowing of Sodium Methoxide Several months ago I mixed NaOH with MeOH in a flask and closed it. Did the same with i-propanol. Th ... |
14-12-2019 at 14:22 by: Pumukli |
Crap from "attempt to make isopropyl salicylate, something interesting happened" Does propene smell like that? I was under the impression that propene is odourless.
Repeat it wit ... |
14-12-2019 at 02:49 by: Pumukli |
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