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Garage Experiments With Trichloromethane.
I was just copying the procedure... It is rather cumbersome to do that, and well good point :D.

T ...
26-4-2005 at 08:08
by: PainKilla
Garage Experiments With Trichloromethane.
Well for ease of use for everyone this translates too:

2 Liter Jar/Flask
1.2L Water
363g 34% B ...
25-4-2005 at 09:29
by: PainKilla
What is the most ignorant thing you have ever done while conducting an experiment?
I think that would be having Caro's acid shooting all over me. I made a batch to see if would d ...
1-4-2005 at 21:16
by: PainKilla
2,6(3,5?)-dinitrophenoxyethyl nitrate
Ok Basically here is what I think happened:

Cl-Bz-Cl ----NaOH> OH-Bz-Cl ------NaOEt> OH- ...
22-3-2005 at 09:03
by: PainKilla
Diphoronepentaperoxide (DPPP)
The thing is he didnt give any results. Theorizing about what COULD happen vs what WILL happen is tw ...
20-3-2005 at 01:56
by: PainKilla
Diphoronepentaperoxide (DPPP)
Before you go critizaing all the hard wrok everyone ahs done, where are YOUR results. I want to see ...
17-3-2005 at 12:41
by: PainKilla
Sodium methoxyde by electrolysis?
I was just reading in my organic chem book that Cl substituion is near impossible without a nitro or ...
17-3-2005 at 12:22
by: PainKilla
Should the Whimsy password be changed?
What does that lnik have to do with anything we aren't making anyone pay us.

Basically, firs ...
6-3-2005 at 18:43
by: PainKilla
Should the Whimsy password be changed?
I think it should be around 20. This way, we know by this time if the member is a kewl or not. Once ...
6-3-2005 at 10:16
by: PainKilla
Bandwidth trouble & images
Why dont you put some sort of donate link, I am sure some members would contribute,as would I.
1-3-2005 at 10:41
by: PainKilla
Download a sciencemadness backup!
My computer is always on due to various things running, and i have a few good progs for downloading ...
24-2-2005 at 19:50
by: PainKilla
Glassware Questions
I have the nylon one, it is just a hole in the top, which is actually slightly big for my thermomete ...
24-2-2005 at 10:37
by: PainKilla
Needed books
Just PM axehandle for an account. Leeching is allowed IIRC, but everyone should upload a thing or tw ...
22-2-2005 at 10:16
by: PainKilla
Diphoronepentaperoxide (DPPP)
I didnt heat and the NaOH was "dyed" an orangish color. I dont think it actually went thro ...
20-2-2005 at 19:06
by: PainKilla
Diphoronepentaperoxide (DPPP)
I just left mine at room temp for a few days. The precipate is NaOH (I used solid NaOH not in soluti ...
20-2-2005 at 17:38
by: PainKilla
Diphoronepentaperoxide (DPPP)
..... Are people missing posts or moreover pages? It was obvious that no Ph-Cl was made when I made ...
15-2-2005 at 15:33
by: PainKilla
Diphoronepentaperoxide (DPPP)
They both lead to the same product. I had a batch of NaOH/acetone and they both formed the red liqui ...
15-2-2005 at 15:12
by: PainKilla
THF ( tetrahydrofuran)
Some things that are pentoses includes:



[url=http://www.biosite.dk/staabi/images/xylan.gif]Xy ...
9-2-2005 at 15:04
by: PainKilla
THF ( tetrahydrofuran)
Was my post totally disregarded? I just mentioned that xylitol is cheap and easily avaialbe from man ...
9-2-2005 at 12:24
by: PainKilla
THF ( tetrahydrofuran)
How interesting, xylitol is a direct derative of xylose, which is a precursor to furfural. Furfural ...
9-2-2005 at 05:30
by: PainKilla
Diphoronepentaperoxide (DPPP)
Well then, thats that :). I guess everyone should thank each other (and especailly rosco) for spendi ...
1-2-2005 at 15:36
by: PainKilla
Diphoronepentaperoxide (DPPP)
No I think it would be a satifactory conclusion to this thread. Unless of course you get MP's t ...
31-1-2005 at 16:03
by: PainKilla
Diphoronepentaperoxide (DPPP)
Joeychemist: You need to dilute the acid before starting anything unless you want an accident like C ...
31-1-2005 at 05:17
by: PainKilla
Diphoronepentaperoxide (DPPP)
I filtered my H2So4 stuff, It looks exactly the same as every describes. I got a good 30-40g estmati ...
30-1-2005 at 17:14
by: PainKilla
Hydroxylamine Production
I didnt say the second reaction did happen, it can though. Also, redcution of ntirogen oxides is to ...
30-1-2005 at 15:20
by: PainKilla
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