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Some experiments in organometallic chemistry
Yes, indeed they are being used. The Pd(dba)2 for Suzuki couplings and other applications where Pd0 ... |
15-5-2009 at 04:26
by: Klute |
Some experiments in organometallic chemistry
I thought I could post a few preparations of organometallic precursors, things I've done lately at w ... |
15-5-2009 at 00:27
by: Klute |
citrates, picrates & oxalates
See my post on oxalates, from dehydrated oxalic acid. I think the same methodology can be applied to ... |
14-5-2009 at 01:06
by: Klute |
Heating Mantle of Hot Plate with oil bath
I think a stirrer is going to be more practical in a first period, you can perform reactions ata var ... |
14-5-2009 at 01:00
by: Klute |
Decomposition of residual peroxides in post reaction mix
I would use thiosulfate, no risk of it reacting with the ketone, and quick reduction of the peroxide ... |
13-5-2009 at 00:52
by: Klute |
Disposal of (old) THF Still
Just take your time adding IPA at first, beware as it takes quite long until bubbling stops completl ... |
13-5-2009 at 00:50
by: Klute |
Synthesis of 3-(p-Hydroxyphenyl)-2-Butanone "raspberry ketone"
I would try using CTH conditions, I requested a few articles on the subject lately, apparently ammon ... |
4-5-2009 at 00:14
by: Klute |
Methylation of phenols with Methyl Nitrate
Yes, if my memory serves right, (MeO)2Ph is easily steam distilled, as an oil that quickly solidifie ... |
21-3-2009 at 04:25
by: Klute |
Synthesis of Pentamethyl Cyclopentadiene
It's a very clever path way, the preparation of the butan-2,3-diol is very clever!
I would directl ... |
19-3-2009 at 00:38
by: Klute |
Methylation of phenols with Methyl Nitrate
Nice work! It's nice to see application to methyl nitrate! Indeed be cautious of storing largish qu ... |
19-3-2009 at 00:27
by: Klute |
HPLC analysis of polar analytes with reverse phase columns
HPLC is a wonderfull science in itself! I'm lacking decent experience with the more sophisticated e ... |
17-3-2009 at 10:40
by: Klute |
HPLC analysis of polar analytes with reverse phase columns
You could try switching to a methanol/H20 system, or even somewhat acidic buffers (phosphate) to "s ... |
16-3-2009 at 13:01
by: Klute |
Ozonelabs: Synthesis of Benzocaine
Very nice! I love your reports!
But why didn't you mention the amount of product collected and th ... |
15-3-2009 at 09:49
by: Klute |
Cinnamamide purification
Thank you very much for the details and the article! That is a reaction I would love to try one day. ... |
5-3-2009 at 02:50
by: Klute |
Material Acquistion (Newbie question)
Thorazine, which country are you in? In most western countries, suppliers do sell glassware to indiv ... |
5-3-2009 at 02:41
by: Klute |
Cinnamamide purification
Isomeric_Fred, could you give us a little detail on the reaction? I'm pretty interested in Heck-like ... |
3-3-2009 at 04:22
by: Klute |
oxalic acid reaction with secondary amines
Very vague, indeed. I guess he is talking about forming the oxalate rather than a tertiary amine tho ... |
28-2-2009 at 12:29
by: Klute |
Peracetic Acid Preparation
Indeed peracetic acid is always in equilibrium with acetic and H2O2, evene when using 30% H2O2 and g ... |
27-2-2009 at 05:47
by: Klute |
Peracetic Acid Preparation
I'm very sceptical that you will get 12% peracetic from 25% AcOH. Could you please details your calc ... |
26-2-2009 at 02:50
by: Klute |
Chemists from France ??
Hehe I guess I'm the guy you are talking about..
Sorry for the late reply, I am indeed moving and ... |
25-2-2009 at 02:58
by: Klute |
cyclopentanone
Benzylchloride, I love the work you do. ALot of intereting reactions. Would have time to make longer ... |
24-2-2009 at 03:32
by: Klute |
thionyl chloride synthesis
Translation of the Compt. Rendus Wurtz paper:
[quote]
INORGANIC CHEMISTRY- Synthesis of thionyl ... |
9-2-2009 at 03:39
by: Klute |
Synthesis of 3-(p-Hydroxyphenyl)-2-Butanone "raspberry ketone"
Thank you 
They really are part of my favourites! Both the smell and the apparence! |
6-2-2009 at 12:30
by: Klute |
Synthesis of 3-(p-Hydroxyphenyl)-2-Butanone "raspberry ketone"
I've stumbled on a pretty interesting article, detailing the use of NiB supported on silica gel to s ... |
6-2-2009 at 03:44
by: Klute |
Solvent Purification
If you are talking about technical grade solvents, and not mixtures, than yes dessicant and distilla ... |
5-2-2009 at 09:47
by: Klute |
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