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Potassium Alum Synthesis from Scrap Aluminium without Sulphuric Acid H2SO4: pKa1 < 0; pKa2 = 1.92
when dissolving Al in H2SO4 the concentration of H3O+ which reacts ... |
2-3-2023 at 10:12 by: Fery |
2,4-DinitrophenylHydrazine Synthesis [Lab Report] Well done!!! Useful reagent for analysis of ketones and aldehydes (Brady's reagent). |
1-3-2023 at 10:40 by: Fery |
aldol condensation of acetone on calcium carbide Deathunter88 you are right, that could be a way to go to separate mesityl oxide. Solubility of mesit ... |
28-2-2023 at 12:31 by: Fery |
95% Ethanol from E85 Fuel E85 is available in CZ too. Cheap. |
28-2-2023 at 03:19 by: Fery |
aldol condensation of acetone on calcium carbide pics distillation (this part should be done differently, but I did not know at that moment)
colum ... |
27-2-2023 at 21:07 by: Fery |
aldol condensation of acetone on calcium carbide pics synthesis:
apparatus, note later I had to replace the dropping funnel with new one as its st ... |
27-2-2023 at 21:01 by: Fery |
aldol condensation of acetone on calcium carbide My goal was to prepare mesityl oxide as I was interested in its scent. Diacetone alcohol does not ha ... |
27-2-2023 at 20:43 by: Fery |
95% Ethanol from E85 Fuel FrankRizzo that's great idea. Pharma ethanol norms are very strict and its purity superior. I'm not ... |
27-2-2023 at 19:28 by: Fery |
95% Ethanol from E85 Fuel I had the same idea few years ago, using distillation column and adjustable variable ratio distillat ... |
26-2-2023 at 10:03 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 Use less acid and bigger flask or put smaller volume into your flask. You can repeatedly add fresh e ... |
24-2-2023 at 04:36 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 alexrandomkat - no tar, no volcano: https://www.sciencemadness.org/whisper/viewthread.php?tid=65311& ... |
23-2-2023 at 21:38 by: Fery |
Acetone condensation with KOH - some experimental results. Isophorone Well done!
I wanted to perform the reaction using CaC2 but not yet time.
https://pubs.rsc.org/en/c ... |
22-2-2023 at 10:53 by: Fery |
Insufficient power for heater - stirrer ? [rquote=681663&tid=159346&author=Sulaiman]My favourite heaters are heating mantles, but they ... |
17-2-2023 at 23:45 by: Fery |
3.5 kg AgNO3 (silver nitrate) for sale [EU] Jeeves225 - your grandpa stored it very well, it is good quality, did not darken and the crystals ar ... |
16-2-2023 at 12:42 by: Fery |
melting point apparatus - ebay Hi dome13, you should return the device and get your money back. I also unscrewed the box to see ins ... |
13-2-2023 at 20:36 by: Fery |
Benzyl alcohol from paint stripper Benzyl alcohol has m.p. -15 C so you can probably freeze it in a common freezer which operates at -1 ... |
6-2-2023 at 21:48 by: Fery |
melting point apparatus - ebay Mateo_swe - exactly. I used Thiele tube with glycerin for years and it was very precise. I wanted to ... |
4-2-2023 at 21:26 by: Fery |
Glacial acetic acid expands on freezing? It does NOT expand of freezing. It shrinks. I have frozen it already few times in original glass bot ... |
26-1-2023 at 20:48 by: Fery |
Fischer synthesis of methyl 3,4,5-trimethoxycinnamate I use 10 ml Dean Stark, it has extra cca 5 ml space above graduation (so totally about 15 ml). So I ... |
26-1-2023 at 20:27 by: Fery |
Fischer synthesis of methyl 3,4,5-trimethoxycinnamate Excellent yield !!! And even at this small scale experiment !!!
After 18 hours the reaction is at e ... |
26-1-2023 at 03:30 by: Fery |
refluxing under a mild vacuum I did [url=https://www.sciencemadness.org/whisper/viewthread.php?tid=64791&goto=search&pid=6 ... |
24-1-2023 at 21:25 by: Fery |
Synthesis of Nitrotoluene SyntheticFunk - well done and welcome here!
o-nitrotoluene must be vacuum distilled through very po ... |
23-1-2023 at 07:05 by: Fery |
Replacement for acetonitrile in oxone oxidation Boffis - maybe due to conjugation couldn't sorbic acid split into propionic acid + malonic acid ??? ... |
22-1-2023 at 05:39 by: Fery |
Replacement for acetonitrile in oxone oxidation Yes of course. The catalyst was pertungstic acid. I dissolved part of 99,6% W TIG welding electrode ... |
21-1-2023 at 23:11 by: Fery |
melting point apparatus - ebay There is a hole to insert own thermometer, there is no digital thermoprobe with display. You can adj ... |
21-1-2023 at 23:04 by: Fery |
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