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Modified Patent Route to Oxalyl Chloride
Merck says nothing about azeotropes. I've found $6/gallon walmart antifreeze to simple distill well, ...
11-4-2007 at 04:16
by: S.C. Wack
The-Hive as torrent
[quote][i]Originally posted by Deevel[/i]
My Mr Wack you are a cheery bugger aren't you? In the int ...
11-4-2007 at 03:54
by: S.C. Wack
Prep of p-Nitrobenzyl Bromide & Relatives
One would think that if much optimization was possible and not a secret, Urbanski would know. Toluen ...
10-4-2007 at 02:06
by: S.C. Wack
sciencelab .com
http://www.bbb.org/

30 complaints in 37 months. Interesting that Strike's SA is within 5 miles of ...
8-4-2007 at 17:26
by: S.C. Wack
The-Hive as torrent
[quote][i]Originally posted by sadhu.ian[/i]
How fucking stupid an american can be? Fucker--don´t ...
6-4-2007 at 13:57
by: S.C. Wack
toluene --> benzaldehyde
The patent says little, as far as I can tell. NiO(OH) is made from a nickel salt + hypochlorite or a ...
5-4-2007 at 04:07
by: S.C. Wack
Acetic anhydride preparation
I had until now forgotten that I have a [url=http://v3.espacenet.com/origdoc?DB=EPODOC&IDX=DE287 ...
1-4-2007 at 02:00
by: S.C. Wack
Acetyl Chloride Watched?
Not on the fed list but I would be not be comfortable being frontierpsychiatrist, the person with th ...
31-3-2007 at 00:48
by: S.C. Wack
help purifying potassium hydroxide (drain cleaner)
Sounds like a product sold at Kmart which does not contain hypochlorite. The amount of dye in that p ...
27-3-2007 at 13:55
by: S.C. Wack
Synthesis of Potassium Hexacyanoferrate(II) i.e. Potassium Ferrocyanide?
A better way IMHO to make it from the usually but not always more expensive ferricyanide is reductio ...
26-3-2007 at 12:28
by: S.C. Wack
Aniline
Maybe you'd like to try using more heat to start with, and different addition strategy such as in Cu ...
25-3-2007 at 14:17
by: S.C. Wack
Acetic anhydride preparation
The abstract strongly suggests that the N2O4 was in the gas phase and does not mention temperature, ...
24-3-2007 at 21:49
by: S.C. Wack
FWIW
Décomposition thermique de l'hypophosphite de sodium
Bulletin de la Société chimique de France
...
24-3-2007 at 10:15
by: S.C. Wack
Acetic anhydride preparation
[quote][i]Originally posted by Sauron[/i]
Kindly stay the hell away from my posts in the future. I ...
24-3-2007 at 05:22
by: S.C. Wack
Controlled Bacterial Nitrification (salpeter production, using nitrosomonas etc)
The stated yield in 100+ year old research (aimed at assuring Chile-dependent France of nitrate shou ...
24-3-2007 at 04:53
by: S.C. Wack
Acetic anhydride preparation
There is nothing wrong with my patent numbers, only the crap sites that you use to look them up.
ht ...
23-3-2007 at 14:43
by: S.C. Wack
Acetic anhydride preparation
Pd may not be necessary with vinyl acetate. See US1856251, which may work as detailed there or not. ...
23-3-2007 at 02:41
by: S.C. Wack
Carboxylic acid -> Alkan
This all depends on what exactly you are trying to decarboxylate. I assume that the COOH is not atta ...
18-3-2007 at 14:45
by: S.C. Wack
analytical machinery
12AX7 - Yes! By all means, let's derail yet another thread with nonsense that could be PM'd if menti ...
17-3-2007 at 04:19
by: S.C. Wack
analytical machinery
That's your fault for using IE or some other crap browser. Looks fine on my monitor.

Stuff that ...
16-3-2007 at 15:32
by: S.C. Wack
Sodium Hydroxide, Drain openers
It is in many jurisdictions. Really.
http://www.kansas.gov/drugenforcement/retailmeth.htm
Programs ...
16-3-2007 at 15:13
by: S.C. Wack
Acetic anhydride preparation
As promised, Gmelin. Its enthusiasm is indeed from that JACS article.

Band 61 B5, Seiten 125-6.
...
15-3-2007 at 02:28
by: S.C. Wack
Zinc powder and potassium nitrate
IIRC I tried both (unactivated) Zn and Mg on conc. solutions sometime in the past;, the only reactio ...
13-3-2007 at 03:56
by: S.C. Wack
Acetic anhydride preparation
Yeah, silver salts are notoriously unrecoverable and unreducable; and scrap silver has no resale val ...
8-3-2007 at 00:30
by: S.C. Wack
Acetic anhydride preparation
Someone else looked into the reaction of silver acetate with CS2, but gave a yield figure this time, ...
7-3-2007 at 04:33
by: S.C. Wack
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