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Bromination of Vanillin without bromine
Hello everyone,

It has been a while since I have posted anything of interest, so I thought I woul ...
23-2-2012 at 22:08
by: mnick12
Cheap, Quality Glass Source (Laboy Glass)
Just a quick update,

I would like to retract my earlier statement about Laboy, it appears as thou ...
22-2-2012 at 18:17
by: mnick12
NaBH4
I know of few places, but it depends where you live.
22-2-2012 at 15:00
by: mnick12
Cheap, Quality Glass Source (Laboy Glass)
Just a word of caution,

I have ordered from Laboy a number of times, through ebay and the the onl ...
18-2-2012 at 10:40
by: mnick12
Good substrate to test Urushibara Nickel?
Yea so far this is looking like it is not going to work.

I tried hydrogenating 1.4ml of nitrobenz ...
26-11-2011 at 21:33
by: mnick12
Good substrate to test Urushibara Nickel?
I have a few ml of eugenol I could try reducing, but I am not quite sure how to test if hydrogenatio ...
17-11-2011 at 17:22
by: mnick12
Good substrate to test Urushibara Nickel?
Just a little update,

Not having any styrene or permanganate, I opted for 4-butoxy-3-methoxypheny ...
16-11-2011 at 18:59
by: mnick12
Good substrate to test Urushibara Nickel?
Hello everyone,

I have a question which I hope some of you may be able to help me with. It has be ...
14-11-2011 at 20:36
by: mnick12
Oxidizing Naphthalene to Phthalic anhydride
Phthalic anhydride? You mean phthalic acid. Anhydrides cannot be precipitated from aqueous solutions ...
31-10-2011 at 18:52
by: mnick12
1-bromo-3-methoxybenzene
I had an interest in this compound a while ago, and while I never completed the synthesis I had good ...
10-10-2011 at 16:26
by: mnick12
4-ethoxyphenol
No I partially neutralized the H2SO4, distilled of 55ml of ethanol, poured the solution into brine t ...
11-9-2011 at 20:50
by: mnick12
4-ethoxyphenol
Hello everyone,
I am having a little bit of trouble with 4-ethoxyphenol. There are a number of thr ...
10-9-2011 at 11:13
by: mnick12
Latest chemical order?
My last orders:

Dimethyl formamide-500ml
Nitromethane-500ml ACS
Methanol-1L
GAA-1L
Methylene ...
8-8-2011 at 19:18
by: mnick12
Request for The Preparation and Testing of Nickel Catalysts for Hydrogenation
Ahhh if your interested in nickel and other transition metal based catalsts there are quite a few fr ...
29-6-2011 at 18:01
by: mnick12
Which is your year of birth?
17 years old, born in 94.
8-6-2011 at 12:39
by: mnick12
Formaldehyde at home - how safe is it?
I have a gallon or so of the stuff in my fridge, and have had it there for about 2 years. So far no ...
6-6-2011 at 13:30
by: mnick12
Preparation of 1-bromo-3-nitrobenzene
I wont be able to do any lab stuff for about 2 months :( , but I will tell some things I did which m ...
4-6-2011 at 19:42
by: mnick12
urea to ammonia to nitrate
There are some species of nitro and nitrosobacter which are able to use urea directly as their nitro ...
13-5-2011 at 19:20
by: mnick12
recution of 1-bromo-3-nitrobenzene
Hello everyone,

I recently prepared a small amount of 1-bromo-3-nitrobenzene from sulfuric acid, ...
1-5-2011 at 13:36
by: mnick12
Preparation of 1-bromo-3-nitrobenzene
Good news, and sorry for the triple post.

Anyway I did a small scale run of the procedure describ ...
1-5-2011 at 13:29
by: mnick12
Making fire (youtube collaborative video)
I dont think recrystallization would work for Ca(ClO)2, hypochlorites are very unstable in aqueous s ...
16-4-2011 at 22:36
by: mnick12
Problems nitrating acetophenone
Hello everyone,
I have an annoying problem that I hope you all may be able to help me with. I am in ...
6-4-2011 at 18:46
by: mnick12
Making fire (youtube collaborative video)
Well if anyone is looking for ideas CrO3 and acetone makes a spectacular fireball-whoooosh if done i ...
27-3-2011 at 13:07
by: mnick12
home brew silica supported hydrogenation catalysts
I've tried urushibara nickel and have had mixed results.

On the subject of nickel oxide I am cert ...
23-3-2011 at 22:11
by: mnick12
Nitroethane from ethylsulfate, Desseigne variation.
Yea its a good idea to use a large excess of ethanol, it makes stirring easier, and the end product ...
22-3-2011 at 20:15
by: mnick12
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