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Nitric Acid Synthesis
[quote]
A catalytic converter will not work, as it is designed to reduce NOx species to N2 and xO2. ...
30-7-2008 at 17:05
by: kilowatt
Nitric Acid Synthesis
You'd need one heck of an ozone generator to oxidize enough ammonia to make significant mole quantit ...
30-7-2008 at 15:16
by: kilowatt
Iodine preparation for who needs it
[quote]
I doubt EVERY iodine compound will be regulated. I am sure there is something we can oxidiz ...
30-7-2008 at 10:24
by: kilowatt
Nitric Acid Synthesis
Well I was thinking of doing it with sulfuric acid. I believe urea nitrate could be liable to explo ...
29-7-2008 at 21:18
by: kilowatt
Nitric Acid Synthesis
It would be easier to just use the NH4NO3 to form metal nitrate and use that to make nitric acid. I ...
29-7-2008 at 21:12
by: kilowatt
Nitric Acid Synthesis
I would react it with a strong alkali first, to yield the corresponding metal nitrate (these are the ...
29-7-2008 at 20:47
by: kilowatt
What reagent would you like to see an illustrated guide for?
Some moderate to high temperature syntheses would be good to see too, and I think they would go well ...
29-7-2008 at 20:33
by: kilowatt
Iodine preparation for who needs it
I can see the restrictions and the disappearance of basic reagents from the consumer market largely ...
29-7-2008 at 15:51
by: kilowatt
What reagent would you like to see an illustrated guide for?
Some very useful reagents that come to mind are thionyl chloride, nitrosyl chloride, PCl5. Even nit ...
28-7-2008 at 20:35
by: kilowatt
Need help w/ Sulfamic synthesis
Not sure about this, but I should think sulfamic acid could be made by the reaction of ammonia with ...
28-7-2008 at 14:53
by: kilowatt
Thunderstorm experiments
Well there's always rocket triggered lightning. That's messing with a LOT of power, though. You ne ...
27-7-2008 at 09:56
by: kilowatt
Iodine preparation for who needs it
I dunno, the city of New York wanted to ban geiger counters.:P And you'd think if people were ever ...
25-7-2008 at 17:59
by: kilowatt
Iodine preparation for who needs it
This is just asking for the DEA to ban KI too. Soon we may all have to resort to the destructive di ...
25-7-2008 at 14:19
by: kilowatt
Contact Process With CO/CO2 Rich Gas
I have collected some lead salt from my sulfating battery and have been assembling the process react ...
22-7-2008 at 18:35
by: kilowatt
artchemicals.com
Looks like they've got some pretty outrageous prices.
18-7-2008 at 16:34
by: kilowatt
The lead salts preparation thread!
That's actually a pole transformer wired for 2400:480. I'm using it at less than 1/20th its rated v ...
17-7-2008 at 14:45
by: kilowatt
The lead salts preparation thread!
I couldn't find my current meter until after I posted this. I did later though, and it's about 15A.
17-7-2008 at 09:41
by: kilowatt
The lead salts preparation thread!
Here is my latest setup for preparing lead sulfate from scrap lead, actually for the separation of t ...
16-7-2008 at 17:48
by: kilowatt
Anhydrous MnCl2 (Mn (II) chloride)?
Try heating the hydrated form strongly under circulating anhydrous HCl gas to prevent hydrolysis. Y ...
16-7-2008 at 10:00
by: kilowatt
Contact Process With CO/CO2 Rich Gas
I need some soft lead for gasket material for my HF retort, so I am getting back to my lead refining ...
15-7-2008 at 20:19
by: kilowatt
trimethyl borate
You could try benzene or toluene. I would think TMB would have a higher affinity for those than met ...
5-7-2008 at 11:29
by: kilowatt
trimethyl borate
Maybe you could distill it with a non-polar solvent to break the azeotrope. There's also vacuum and ...
5-7-2008 at 11:19
by: kilowatt
ruined crucible
When a metal or alloy of known melting point is melting, that's the temperature you've got. If you ...
1-7-2008 at 17:42
by: kilowatt
Condensing chlorine gas, price of ethane!!!!
H2SO4 is an extremely powerful dessicant. It is used to remove water from gases like chlorine or HC ...
30-6-2008 at 16:26
by: kilowatt
Unified Copper Process
[quote]
Then mix the solid bromate SLOWLY with concentrated NaBr acidulated with H2SO4... This can ...
30-6-2008 at 14:47
by: kilowatt
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