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Forget everything else, diamond is the answer!
Hmmm, well the oxygen for the perchlorate comes from the water so I don't know what would happen wit ...
9-1-2008 at 04:58
by: jpsmith123
Electrodeposition Of Diamond-Like Films
I found an interesting abstract of a thesis (couldn't get the paper though):

Diamond-Like Carbon ...
8-1-2008 at 17:26
by: jpsmith123
Forget everything else, diamond is the answer!
IIRC it starts to oxidize around 700 C or something like that, so you're probably better off with pl ...
8-1-2008 at 14:57
by: jpsmith123
Here's another interesting paper.
This paper describes some diamond coated anodes. Note the current densities they tested them at.

...
8-1-2008 at 12:47
by: jpsmith123
Forget everything else, diamond is the answer!
@-jeffB: Thanks for the reference. I've posted a request for the full paper.

@microcosmicus: Theo ...
8-1-2008 at 08:11
by: jpsmith123
Forget everything else, diamond is the answer!
I'm still thinking about this, especially since none of other efforts have yet produced a reliable p ...
8-1-2008 at 07:10
by: jpsmith123
Perchlorate manufacture (not) with Graphite
Well I sanded my piece of Ti with 220 grit SiC paper, washed it with detergent solution, cathodized ...
4-1-2008 at 05:59
by: jpsmith123
KCLO3 by way of H2O + KCL
Did you see the rest of their catalog [url=http://www.jumpinjackflashpyrosupplies.com/servlet/the-St ...
4-1-2008 at 05:40
by: jpsmith123
Cobalt Oxide Anodes
This wire had a layer of Co cathodically electrodeposited onto it from Co acetate & vinegar solu ...
3-1-2008 at 06:54
by: jpsmith123
Perchlorate manufacture (not) with Graphite
I was able to plate cobalt onto Ti by hydriding it first...and patent #4127709 claims to accomplishe ...
3-1-2008 at 06:52
by: jpsmith123
Perchlorate manufacture (not) with Graphite
Sorry to hear the Pt didn't stick. I know the feeling. I wonder if electrocleaning or hydriding of t ...
3-1-2008 at 05:24
by: jpsmith123
Drying Molecular Sieve in a Microwave Oven
Hi Solo,

Thanks for the interesting paper. Although it's not primarily concerned with drying, it ...
27-12-2007 at 19:06
by: jpsmith123
Drying Molecular Sieve in a Microwave Oven
I'm wondering, has anyone ever tried to dry any flavor of zeolite in a microwave, and if so how well ...
27-12-2007 at 17:24
by: jpsmith123
My Chlorate Cell
Your cell looks pretty good there, Xenoid.

Attached is a picture of mine.

The container is a 4 ...
21-12-2007 at 18:21
by: jpsmith123
Tin Oxide + Antimony Oxide Anode
I wonder if the SnO2 - Sb2O3 - Bi2O3 - etc. film could be made from a gas-flame-oxidized metal film? ...
19-12-2007 at 18:41
by: jpsmith123
Tin Oxide + Antimony Oxide Anode
I'm surprised an electronics place has it. Over here it's mainly used for plumbing applications. And ...
19-12-2007 at 17:33
by: jpsmith123
Tin Oxide + Antimony Oxide Anode
Well being that Christmas is coming, I think Dann2 just needs to get her something special...like ma ...
19-12-2007 at 16:38
by: jpsmith123
Tin Oxide + Antimony Oxide Anode
Well Dann2 today I tried to buy some 95/5 solder locally, and I couldn't find any; Lowe's didn't hav ...
19-12-2007 at 14:04
by: jpsmith123
Tin Oxide + Antimony Oxide Anode
Just wondering, has anyone been able to use OTC 95/5 solder to make a suitable precursor for a pyrol ...
18-12-2007 at 05:45
by: jpsmith123
Forget everything else, diamond is the answer!
I'd bet that you could use a graphite substrate with the surface prepared by anodic etching in NaOH, ...
17-12-2007 at 05:54
by: jpsmith123
Forget everything else, diamond is the answer!
I've seen a patent claiming that you can use water/alcohol vapor instead of H2 & CH4.

But any ...
16-12-2007 at 15:26
by: jpsmith123
Lithium (Per)Chlorate cell
Perhaps Dann2 was referring to the attached patent.
15-12-2007 at 18:17
by: jpsmith123
Cobalt Oxide Anodes
Dann2 the Co Oxide coated anodes you're referring to, are they baked on coatings or electrodeposited ...
14-12-2007 at 16:22
by: jpsmith123
Dosivac Vacuum Pump
I've just about given up on my hope of someday finding a dry scroll pump like an Edwards XDS10 cheap ...
14-12-2007 at 08:45
by: jpsmith123
Cobalt Oxide Anodes
Anybody that has some Mn Sulfate and Co Sulfate might want to try anodic co-electrodeposition of the ...
13-12-2007 at 13:44
by: jpsmith123
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