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2,3,5,6-Tetraazidobenzoquinone
Hydrazinium nitranilate & other high-density energetic nitranilates:

http://www3.interscience ...
27-12-2008 at 13:59
by: Taoiseach
2,3,5,6-Tetraazidobenzoquinone
I just made some chloranil from paracetamol+NH4NO3+HCl. It worked niceley, altough the product is co ...
27-12-2008 at 05:47
by: Taoiseach
Peroxymanganates
According to the paper (if I understand correctly), the well-known catalytic decomposition of H2O2 w ...
10-12-2008 at 00:21
by: Taoiseach
Peroxymanganates
Ammonium peroxymanganate is mentioned in the Hazardous Chemicals Handbook.

Also, peroxymanganates ...
9-12-2008 at 08:01
by: Taoiseach
Silver Precipitation from Silver Nitrite
@Jor

I precipated silver powder from AgCl some time ago and run into similar problems. AgCl tends ...
6-12-2008 at 03:22
by: Taoiseach
Silver Precipitation from Silver Nitrite
Boil with NaOH and cane sugar. That will precipate Ag as a fine powder. Wash with water and dry in w ...
4-12-2008 at 13:24
by: Taoiseach
Benzoic Acid, Carbamid>Benzamid>Anilin?
Awesome work smuv, thanks for sharing!

:cool:
1-12-2008 at 23:22
by: Taoiseach
Kits for Sulphuric and Nitric acids
I wonder if an ordinary steel pipe would work as a reaction vessel too. Certainly steel doesnt survi ...
27-11-2008 at 00:52
by: Taoiseach
Nitrourea salts as primaries
Video of H2N-CO-N-NO2.Ag (silvernitrocarbamide) deflagrating:

http://geocities.com/roguemovies7/i ...
23-11-2008 at 03:40
by: Taoiseach
Nitrourea salts as primaries
Nitrourea being acidic forms salts with various bases. The silver and mercury salts are said to be s ...
22-11-2008 at 15:58
by: Taoiseach
Ozonides
NaO3 stable at room temp is claimed to be prepared by passing O3 over dry NaOH:
http://ntrs.nasa.go ...
22-11-2008 at 14:53
by: Taoiseach
Ozonides
Check this out:

http://ozonatedoliveoil.com/
http://www.journalarchive.jst.go.jp/jnlpdf.php?cdjo ...
22-11-2008 at 12:59
by: Taoiseach
Check out attachment
This is the most interesting part. Check out the lower left part of the graph, starting from CrO4((2 ...
21-11-2008 at 07:44
by: Taoiseach
Write-up on synthesis of K3CrO8, a very energetic peroxochromate
Here's by far the most comprehensive treatise on peroxo metallates:

http://ir.lib.sfu.ca/bitstrea ...
21-11-2008 at 07:17
by: Taoiseach
Any explosives made with Napthalene?
@Axt

The Naphthalene diozonide looks interesting.
Have you tried making potassium ozonide? I ha ...
11-11-2008 at 00:03
by: Taoiseach
2,3,5,6-Tetraazidobenzoquinone
There it is :)

Unfortunately no synthesis is given, only a reference to Berichte der Deutsche Che ...
9-11-2008 at 08:00
by: Taoiseach
2,3,5,6-Tetraazidobenzoquinone
Ammonium nitranilate. Also sheds some light on the bonding/structure in nitralinic acid:

http://j ...
9-11-2008 at 03:55
by: Taoiseach
Electrolytic Production of Sulphuric Acid + some questions.
Awesome work again, DerAlte! Does this work with FeSO4 or Na2SO4 too? The latter is tempting because ...
19-10-2008 at 10:09
by: Taoiseach
Halogenated Amines - the others
Does N-tetrabromoethylenediamine work as a complexing agent? I figure each of the 4 N atoms has a lo ...
19-10-2008 at 09:55
by: Taoiseach
HClO3 from Pb(ClO3)2 + H2SO4
You can boil NaCl out of a NaCl/NaClO3 solution. I have done this sucessfully to purify NaClO3. The ...
6-10-2008 at 22:56
by: Taoiseach
Permanganates
Nope it doesn't give the preparation from MnO2 but from the hydrate. Which is not the stuff you can ...
16-9-2008 at 22:31
by: Taoiseach
Hydrogen Peroxide Production
I should do some calculations before posting shit like my previous post :mad:
Actually its not that ...
12-9-2008 at 14:13
by: Taoiseach
Acetonitrile form Ammonium acetate
urea with acetic acid

Is acetic anhydride necessary for this reaction to work?
8-9-2008 at 23:30
by: Taoiseach
Hydrogen Peroxide Production
I know there're threads on this already but just wanted to bring this up because nobody seems to hav ...
8-9-2008 at 08:14
by: Taoiseach
The lead salts preparation thread!
[quote]Back regarding this method, as I stated before fusing a large quantity of ammonium nitrate an ...
16-8-2008 at 03:23
by: Taoiseach
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