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Somewhat Unusual Properties of Ammonium Benzoate [rquote=672138&tid=158476&author=hodges][rquote=672134&tid=158476&author=SplendidAcy ... |
22-3-2022 at 03:10 by: SplendidAcylation |
Is trichloroisocyanuric acid actually an acid? Thanks for the replies!
The pKa of cyanuric acid seems to be about 7 according to this:
[url]htt ... |
22-3-2022 at 03:03 by: SplendidAcylation |
Conversion of APAAN(α-phenylacetoacetonitrile) into BMK It's interesting that it's so easy to decarboxylate the intermediate carboxylic acid simply by heati ... |
22-3-2022 at 02:50 by: SplendidAcylation |
Somewhat Unusual Properties of Ammonium Benzoate That's interesting!
Is there any particular reason you recrystallized the benzoic acid from acetone ... |
20-3-2022 at 06:05 by: SplendidAcylation |
Is trichloroisocyanuric acid actually an acid? Wikipedia (famous for its trustworthiness) states:
"Salts of trichloroisocyanuric acid are known as ... |
13-3-2022 at 03:26 by: SplendidAcylation |
Frustration with trying to make ammonium formate I made some a while ago, I can't remember exactly how the reaction progressed, but it went quite wel ... |
14-8-2021 at 14:06 by: SplendidAcylation |
simple preparation for iminium/eschenmoser salts for the mannich Fantastic ![:)](./images/smilies/smile.gif)
I shall be trying this myself some time soon.
Its nice to see that the dimethylamine ... |
10-8-2021 at 02:25 by: SplendidAcylation |
Steven's Rearrangement - Alternative strong bases to NaNH2
Thanks for the replies!
I bring news of success...
@karlos
I think potassium tert butoxide wa ... |
2-9-2020 at 16:14 by: SplendidAcylation |
Can you make methanol from formic acid? [rquote=640426&tid=155776&author=Junk_Enginerd][rquote=640415&tid=155776&author=Alko ... |
11-7-2020 at 15:22 by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure [rquote=640418&tid=155748&author=Tsjerk]Benzoic acid is not soluble in benzaldehyde, so it w ... |
11-7-2020 at 12:50 by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure Thanks for the replies!
I have got it to work.
I left it overnight after the initial (failed) at ... |
11-7-2020 at 11:35 by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure Hi,
Today I attempted the much awaited synthesis of benzoin... Well, it is much awaited by me, as ... |
7-7-2020 at 17:50 by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide? I'm sorry, I thought I had responded to all of the posts here ![:o](./images/smilies/shocked.gif)
@woelen, thanks for the advice, ... |
5-7-2020 at 17:24 by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving [rquote=639625&tid=155696&author=DraconicAcid][rquote=639624&tid=155696&author=Splen ... |
1-7-2020 at 17:47 by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving Thanks for the replies everyone!
[rquote=639583&tid=155696&author=woelen]With increasin ... |
1-7-2020 at 13:37 by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving Hi
I have recently acquired some sodium metal, with which I intend to make an anhydrous superbase ... |
30-6-2020 at 17:36 by: SplendidAcylation |
Why is tin and HCl rxn so slow? [rquote=639352&tid=155674&author=DraconicAcid][rquote=639350&tid=155674&author=Splen ... |
29-6-2020 at 17:06 by: SplendidAcylation |
Why is tin and HCl rxn so slow? I did this reaction recently
It is indeed very slow, I reasoned that it is because of tin's posit ... |
27-6-2020 at 17:30 by: SplendidAcylation |
Steven's Rearrangement - Alternative strong bases to NaNH2 Hi
Having been scheming about the synthesis of N,N-dimethyl-1,2-diphenylethylamine for many month ... |
27-6-2020 at 10:28 by: SplendidAcylation |
Disappointing results with 3A molecular sieves I tried the same thing with sieves bought from China
Something like:
Sieves were first weighe ... |
22-6-2020 at 09:47 by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide? [rquote=637385&tid=155502&author=DavidJR]Found online:
(From http://www.chem.latech.edu/ ... |
4-6-2020 at 18:02 by: SplendidAcylation |
Synthesis of benzonitrile by P2O5 dehydration of benzamide - another perplexing failure [rquote=637368&tid=155509&author=clearly_not_atara]As P2O5 is hydrated, it converts to metap ... |
4-6-2020 at 17:57 by: SplendidAcylation |
ethyl formate - esterification by reactive distillation Fantastic.
Thanks for taking the time to write this up.
I think I might give it a try, but I onl ... |
1-6-2020 at 18:01 by: SplendidAcylation |
Synthesis of benzonitrile by P2O5 dehydration of benzamide - another perplexing failure Another addition to the fail collection!
A few months ago, I got quite excited when I found out t ... |
1-6-2020 at 17:47 by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide? Thanks for all the replies.
Looks like thiamine is the way to go, although I'll probably end up t ... |
1-6-2020 at 17:10 by: SplendidAcylation |
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